6,6-[Ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one

The title compound, C(19)H(22)N(2)O(2)S(2), consists of a tetra­cyclic ring system containing an azocine skeleton with methoxy­ethyl and dithiol­ane groups as substituents. The benzene and five-membered N-heterocyclic rings are nearly coplanar, making a dihedral angle of 0.81 (12)°. The dithiol­ane...

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Detalles Bibliográficos
Autores principales: Tercan, Barış, Yüksel, Fatma, Patır, Süleyman, Hökelek, Tuncer
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979528/
https://www.ncbi.nlm.nih.gov/pubmed/21579376
http://dx.doi.org/10.1107/S1600536810015941
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author Tercan, Barış
Yüksel, Fatma
Patır, Süleyman
Hökelek, Tuncer
author_facet Tercan, Barış
Yüksel, Fatma
Patır, Süleyman
Hökelek, Tuncer
author_sort Tercan, Barış
collection PubMed
description The title compound, C(19)H(22)N(2)O(2)S(2), consists of a tetra­cyclic ring system containing an azocine skeleton with methoxy­ethyl and dithiol­ane groups as substituents. The benzene and five-membered N-heterocyclic rings are nearly coplanar, making a dihedral angle of 0.81 (12)°. The dithiol­ane ring adopts an envelope conformation. Inter­molecular N—H⋯O hydrogen-bonding and weak C—H⋯π inter­actions are present in the crystal structure.
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spelling pubmed-29795282010-12-30 6,6-[Ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one Tercan, Barış Yüksel, Fatma Patır, Süleyman Hökelek, Tuncer Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(19)H(22)N(2)O(2)S(2), consists of a tetra­cyclic ring system containing an azocine skeleton with methoxy­ethyl and dithiol­ane groups as substituents. The benzene and five-membered N-heterocyclic rings are nearly coplanar, making a dihedral angle of 0.81 (12)°. The dithiol­ane ring adopts an envelope conformation. Inter­molecular N—H⋯O hydrogen-bonding and weak C—H⋯π inter­actions are present in the crystal structure. International Union of Crystallography 2010-05-08 /pmc/articles/PMC2979528/ /pubmed/21579376 http://dx.doi.org/10.1107/S1600536810015941 Text en © Tercan et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Tercan, Barış
Yüksel, Fatma
Patır, Süleyman
Hökelek, Tuncer
6,6-[Ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one
title 6,6-[Ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one
title_full 6,6-[Ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one
title_fullStr 6,6-[Ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one
title_full_unstemmed 6,6-[Ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one
title_short 6,6-[Ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one
title_sort 6,6-[ethyl­enebis(sulfanediyl)]-2-(2-methoxy­ethyl)-1,2,3,4,5,6-hexa­hydro-1,5-methano-1h-azocino[4,3-b]indol-3-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979528/
https://www.ncbi.nlm.nih.gov/pubmed/21579376
http://dx.doi.org/10.1107/S1600536810015941
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AT hokelektuncer 66ethylenebissulfanediyl22methoxyethyl123456hexahydro15methano1hazocino43bindol3one

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