1-(2-Bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate

In the crystal of the title compound, C(8)H(17)BrN(2) (2+)·Br(−)·BF(4) (−), a weak inter­molecular N—H⋯Br hydrogen bond is observed between the cation and the bromide anion. A two-part disorder model was applied to the BF(4) (−) anion with a refined major–minor occupancy ratio of 0.837 (14):0.163 (1...

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Detalles Bibliográficos
Autor principal: Xiao, Jing-mei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979572/
https://www.ncbi.nlm.nih.gov/pubmed/21579433
http://dx.doi.org/10.1107/S1600536810017204
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author Xiao, Jing-mei
author_facet Xiao, Jing-mei
author_sort Xiao, Jing-mei
collection PubMed
description In the crystal of the title compound, C(8)H(17)BrN(2) (2+)·Br(−)·BF(4) (−), a weak inter­molecular N—H⋯Br hydrogen bond is observed between the cation and the bromide anion. A two-part disorder model was applied to the BF(4) (−) anion with a refined major–minor occupancy ratio of 0.837 (14):0.163 (14).
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spelling pubmed-29795722010-12-30 1-(2-Bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate Xiao, Jing-mei Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal of the title compound, C(8)H(17)BrN(2) (2+)·Br(−)·BF(4) (−), a weak inter­molecular N—H⋯Br hydrogen bond is observed between the cation and the bromide anion. A two-part disorder model was applied to the BF(4) (−) anion with a refined major–minor occupancy ratio of 0.837 (14):0.163 (14). International Union of Crystallography 2010-05-15 /pmc/articles/PMC2979572/ /pubmed/21579433 http://dx.doi.org/10.1107/S1600536810017204 Text en © Jing-mei Xiao 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Xiao, Jing-mei
1-(2-Bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate
title 1-(2-Bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate
title_full 1-(2-Bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate
title_fullStr 1-(2-Bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate
title_full_unstemmed 1-(2-Bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate
title_short 1-(2-Bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate
title_sort 1-(2-bromo­ethyl)-1,4-diazo­niabicyclo­[2.2.2]octane bromide tetra­fluoro­borate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979572/
https://www.ncbi.nlm.nih.gov/pubmed/21579433
http://dx.doi.org/10.1107/S1600536810017204
work_keys_str_mv AT xiaojingmei 12bromoethyl14diazoniabicyclo222octanebromidetetrafluoroborate

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