1,10-Phenanthroline–dithio­oxamide (2/1)

The asymmetric unit of the title compound, C(12)H(8)N(2)·0.5C(2)H(4)N(2)S(2), contains one 1,10-phenanthroline mol­ecule and a half-mol­ecule of dithio­oxamide, which lies across a crystallographic inversion center. The 1,10-phenanthroline unit is not strictly planar, with dihedral angles between th...

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Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Loh, Wan-Sin, Maity, Annada C., Goswami, Shyamaprosad
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979584/
https://www.ncbi.nlm.nih.gov/pubmed/21579413
http://dx.doi.org/10.1107/S1600536810016405
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author Fun, Hoong-Kun
Loh, Wan-Sin
Maity, Annada C.
Goswami, Shyamaprosad
author_facet Fun, Hoong-Kun
Loh, Wan-Sin
Maity, Annada C.
Goswami, Shyamaprosad
author_sort Fun, Hoong-Kun
collection PubMed
description The asymmetric unit of the title compound, C(12)H(8)N(2)·0.5C(2)H(4)N(2)S(2), contains one 1,10-phenanthroline mol­ecule and a half-mol­ecule of dithio­oxamide, which lies across a crystallographic inversion center. The 1,10-phenanthroline unit is not strictly planar, with dihedral angles between the central benzene ring and the pyridine rings of 1.42 (10) and 1.40 (10)°. In the crystal structure, two 1,10-phenanthroline mol­ecules are linked together by one dithio­oxamide via inter­molecular N—H⋯N hydrogen bonds.
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spelling pubmed-29795842010-12-30 1,10-Phenanthroline–dithio­oxamide (2/1) Fun, Hoong-Kun Loh, Wan-Sin Maity, Annada C. Goswami, Shyamaprosad Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(12)H(8)N(2)·0.5C(2)H(4)N(2)S(2), contains one 1,10-phenanthroline mol­ecule and a half-mol­ecule of dithio­oxamide, which lies across a crystallographic inversion center. The 1,10-phenanthroline unit is not strictly planar, with dihedral angles between the central benzene ring and the pyridine rings of 1.42 (10) and 1.40 (10)°. In the crystal structure, two 1,10-phenanthroline mol­ecules are linked together by one dithio­oxamide via inter­molecular N—H⋯N hydrogen bonds. International Union of Crystallography 2010-05-12 /pmc/articles/PMC2979584/ /pubmed/21579413 http://dx.doi.org/10.1107/S1600536810016405 Text en © Fun et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Loh, Wan-Sin
Maity, Annada C.
Goswami, Shyamaprosad
1,10-Phenanthroline–dithio­oxamide (2/1)
title 1,10-Phenanthroline–dithio­oxamide (2/1)
title_full 1,10-Phenanthroline–dithio­oxamide (2/1)
title_fullStr 1,10-Phenanthroline–dithio­oxamide (2/1)
title_full_unstemmed 1,10-Phenanthroline–dithio­oxamide (2/1)
title_short 1,10-Phenanthroline–dithio­oxamide (2/1)
title_sort 1,10-phenanthroline–dithio­oxamide (2/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979584/
https://www.ncbi.nlm.nih.gov/pubmed/21579413
http://dx.doi.org/10.1107/S1600536810016405
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AT lohwansin 110phenanthrolinedithiooxamide21
AT maityannadac 110phenanthrolinedithiooxamide21
AT goswamishyamaprosad 110phenanthrolinedithiooxamide21

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