2-[2-(2,6-Dichloro­anilino)phen­yl]-N′-(4-propyl­cyclo­hexyl­idene)acetohydrazide

The asymmetric unit of the title compound, C(23)H(27)Cl(2)N(3)O, contains two crystallographically independent mol­ecules in which the dihedral angles between the benzene rings are 70.1 (3) and 63.8 (3)°. In each mol­ecule an intra­molecular N—H⋯O hydrogen bond generates an S(7) ring. The atoms of t...

Descripción completa

Detalles Bibliográficos
Autores principales: Akkurt, Mehmet, Nassozi, Mebble, Çapan, Gültaze, Kocabalkanlı, Ayşe, Çelik, Ísmail, Büyükgüngör, Orhan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979672/
https://www.ncbi.nlm.nih.gov/pubmed/21579699
http://dx.doi.org/10.1107/S1600536809054695
_version_ 1782191469491126272
author Akkurt, Mehmet
Nassozi, Mebble
Çapan, Gültaze
Kocabalkanlı, Ayşe
Çelik, Ísmail
Büyükgüngör, Orhan
author_facet Akkurt, Mehmet
Nassozi, Mebble
Çapan, Gültaze
Kocabalkanlı, Ayşe
Çelik, Ísmail
Büyükgüngör, Orhan
author_sort Akkurt, Mehmet
collection PubMed
description The asymmetric unit of the title compound, C(23)H(27)Cl(2)N(3)O, contains two crystallographically independent mol­ecules in which the dihedral angles between the benzene rings are 70.1 (3) and 63.8 (3)°. In each mol­ecule an intra­molecular N—H⋯O hydrogen bond generates an S(7) ring. The atoms of the propyl grouping of one mol­ecule are disordered over two orientations with occupancies of 0.666 (6) and 0.334 (6). The crystal structure is stabilized by N—H⋯O and C—H⋯O hydrogen-bonding inter­actions.
format Text
id pubmed-2979672
institution National Center for Biotechnology Information
language English
publishDate 2010
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29796722010-12-30 2-[2-(2,6-Dichloro­anilino)phen­yl]-N′-(4-propyl­cyclo­hexyl­idene)acetohydrazide Akkurt, Mehmet Nassozi, Mebble Çapan, Gültaze Kocabalkanlı, Ayşe Çelik, Ísmail Büyükgüngör, Orhan Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(23)H(27)Cl(2)N(3)O, contains two crystallographically independent mol­ecules in which the dihedral angles between the benzene rings are 70.1 (3) and 63.8 (3)°. In each mol­ecule an intra­molecular N—H⋯O hydrogen bond generates an S(7) ring. The atoms of the propyl grouping of one mol­ecule are disordered over two orientations with occupancies of 0.666 (6) and 0.334 (6). The crystal structure is stabilized by N—H⋯O and C—H⋯O hydrogen-bonding inter­actions. International Union of Crystallography 2010-01-09 /pmc/articles/PMC2979672/ /pubmed/21579699 http://dx.doi.org/10.1107/S1600536809054695 Text en © Akkurt et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Akkurt, Mehmet
Nassozi, Mebble
Çapan, Gültaze
Kocabalkanlı, Ayşe
Çelik, Ísmail
Büyükgüngör, Orhan
2-[2-(2,6-Dichloro­anilino)phen­yl]-N′-(4-propyl­cyclo­hexyl­idene)acetohydrazide
title 2-[2-(2,6-Dichloro­anilino)phen­yl]-N′-(4-propyl­cyclo­hexyl­idene)acetohydrazide
title_full 2-[2-(2,6-Dichloro­anilino)phen­yl]-N′-(4-propyl­cyclo­hexyl­idene)acetohydrazide
title_fullStr 2-[2-(2,6-Dichloro­anilino)phen­yl]-N′-(4-propyl­cyclo­hexyl­idene)acetohydrazide
title_full_unstemmed 2-[2-(2,6-Dichloro­anilino)phen­yl]-N′-(4-propyl­cyclo­hexyl­idene)acetohydrazide
title_short 2-[2-(2,6-Dichloro­anilino)phen­yl]-N′-(4-propyl­cyclo­hexyl­idene)acetohydrazide
title_sort 2-[2-(2,6-dichloro­anilino)phen­yl]-n′-(4-propyl­cyclo­hexyl­idene)acetohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979672/
https://www.ncbi.nlm.nih.gov/pubmed/21579699
http://dx.doi.org/10.1107/S1600536809054695
work_keys_str_mv AT akkurtmehmet 2226dichloroanilinophenyln4propylcyclohexylideneacetohydrazide
AT nassozimebble 2226dichloroanilinophenyln4propylcyclohexylideneacetohydrazide
AT capangultaze 2226dichloroanilinophenyln4propylcyclohexylideneacetohydrazide
AT kocabalkanlıayse 2226dichloroanilinophenyln4propylcyclohexylideneacetohydrazide
AT celikismail 2226dichloroanilinophenyln4propylcyclohexylideneacetohydrazide
AT buyukgungororhan 2226dichloroanilinophenyln4propylcyclohexylideneacetohydrazide

Ejemplares similares