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[3-(Iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate

The title compound, C(23)H(24)INOP(+)·C(24)H(20)B(−), was prepared by treatment of 3-amino­propyl triphenyl­phospho­nium bromide hydrogen bromide with p-nitro­phenyl iodo­acetate at 203 K. The asymmetric unit contains a single cation and anion, which are linked in the crystal by inter­molecular N—H⋯...

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Detalles Bibliográficos
Autor principal: Evans, Cameron
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979758/
https://www.ncbi.nlm.nih.gov/pubmed/21579806
http://dx.doi.org/10.1107/S160053681000142X
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author Evans, Cameron
author_facet Evans, Cameron
author_sort Evans, Cameron
collection PubMed
description The title compound, C(23)H(24)INOP(+)·C(24)H(20)B(−), was prepared by treatment of 3-amino­propyl triphenyl­phospho­nium bromide hydrogen bromide with p-nitro­phenyl iodo­acetate at 203 K. The asymmetric unit contains a single cation and anion, which are linked in the crystal by inter­molecular N—H⋯π and inversion-related R (2) (2)(14) C—H⋯O inter­actions, which combine to form chains of cations and anions along the c axis.
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spelling pubmed-29797582010-12-30 [3-(Iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate Evans, Cameron Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(23)H(24)INOP(+)·C(24)H(20)B(−), was prepared by treatment of 3-amino­propyl triphenyl­phospho­nium bromide hydrogen bromide with p-nitro­phenyl iodo­acetate at 203 K. The asymmetric unit contains a single cation and anion, which are linked in the crystal by inter­molecular N—H⋯π and inversion-related R (2) (2)(14) C—H⋯O inter­actions, which combine to form chains of cations and anions along the c axis. International Union of Crystallography 2010-01-16 /pmc/articles/PMC2979758/ /pubmed/21579806 http://dx.doi.org/10.1107/S160053681000142X Text en © Cameron Evans 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Evans, Cameron
[3-(Iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate
title [3-(Iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate
title_full [3-(Iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate
title_fullStr [3-(Iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate
title_full_unstemmed [3-(Iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate
title_short [3-(Iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate
title_sort [3-(iodo­acetamido)prop­yl]triphenyl­phospho­nium tetra­phenyl­borate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979758/
https://www.ncbi.nlm.nih.gov/pubmed/21579806
http://dx.doi.org/10.1107/S160053681000142X
work_keys_str_mv AT evanscameron 3iodoacetamidopropyltriphenylphosphoniumtetraphenylborate