(E)-5-(3,5-Dimethyl­phen­yl)-N-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine

The title compound, C(18)H(17)N(3)S(2), was synthesized by the reaction of 5-(3,5-dimethyl­phen­yl)-1,3,4-thia­diazol-2-amine and 4-(methyl­sulfan­yl)benzaldehyde. An intra­molecular C—H⋯S hydrogen bond results in the formation of a planar (r.m.s. deviation = 0.003 Å) five-membered ring. In the crys...

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Detalles Bibliográficos
Autores principales: Hu, Jun, Ji, Jin-xiu, Zhou, Ying, Wang, Ji-kui, Xu, Yan-hua
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979762/
https://www.ncbi.nlm.nih.gov/pubmed/21579829
http://dx.doi.org/10.1107/S1600536810001558
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author Hu, Jun
Ji, Jin-xiu
Zhou, Ying
Wang, Ji-kui
Xu, Yan-hua
author_facet Hu, Jun
Ji, Jin-xiu
Zhou, Ying
Wang, Ji-kui
Xu, Yan-hua
author_sort Hu, Jun
collection PubMed
description The title compound, C(18)H(17)N(3)S(2), was synthesized by the reaction of 5-(3,5-dimethyl­phen­yl)-1,3,4-thia­diazol-2-amine and 4-(methyl­sulfan­yl)benzaldehyde. An intra­molecular C—H⋯S hydrogen bond results in the formation of a planar (r.m.s. deviation = 0.003 Å) five-membered ring. In the crystal structure, inter­molecular C—H⋯N hydrogen bonds link the mol­ecules to form layers parallel to (011).
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spelling pubmed-29797622010-12-30 (E)-5-(3,5-Dimethyl­phen­yl)-N-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine Hu, Jun Ji, Jin-xiu Zhou, Ying Wang, Ji-kui Xu, Yan-hua Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(17)N(3)S(2), was synthesized by the reaction of 5-(3,5-dimethyl­phen­yl)-1,3,4-thia­diazol-2-amine and 4-(methyl­sulfan­yl)benzaldehyde. An intra­molecular C—H⋯S hydrogen bond results in the formation of a planar (r.m.s. deviation = 0.003 Å) five-membered ring. In the crystal structure, inter­molecular C—H⋯N hydrogen bonds link the mol­ecules to form layers parallel to (011). International Union of Crystallography 2010-01-20 /pmc/articles/PMC2979762/ /pubmed/21579829 http://dx.doi.org/10.1107/S1600536810001558 Text en © Hu et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hu, Jun
Ji, Jin-xiu
Zhou, Ying
Wang, Ji-kui
Xu, Yan-hua
(E)-5-(3,5-Dimethyl­phen­yl)-N-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine
title (E)-5-(3,5-Dimethyl­phen­yl)-N-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine
title_full (E)-5-(3,5-Dimethyl­phen­yl)-N-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine
title_fullStr (E)-5-(3,5-Dimethyl­phen­yl)-N-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine
title_full_unstemmed (E)-5-(3,5-Dimethyl­phen­yl)-N-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine
title_short (E)-5-(3,5-Dimethyl­phen­yl)-N-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine
title_sort (e)-5-(3,5-dimethyl­phen­yl)-n-[4-(methyl­sulfan­yl)benzyl­idene]-1,3,4-thia­diazol-2-amine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979762/
https://www.ncbi.nlm.nih.gov/pubmed/21579829
http://dx.doi.org/10.1107/S1600536810001558
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