2,4,6,8-Tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one

In the title compound, C(31)H(24)Br(4)N(2)O, one of the bromo­phenyl rings is disordered over two orientations with occupancies of 0.69 (2) and 0.31 (2). The bicyclo­[3.3.1]nonane ring system adopts a chair–boat conformation. In the crystal structure, mol­ecules are linked into chains along the c ax...

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Autores principales: Loh, Wan-Sin, Fun, Hoong-Kun, Sarveswari, S., Vijayakumar, V., Reddy, B. Palakshi
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979866/
https://www.ncbi.nlm.nih.gov/pubmed/21579706
http://dx.doi.org/10.1107/S1600536809055226
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author Loh, Wan-Sin
Fun, Hoong-Kun
Sarveswari, S.
Vijayakumar, V.
Reddy, B. Palakshi
author_facet Loh, Wan-Sin
Fun, Hoong-Kun
Sarveswari, S.
Vijayakumar, V.
Reddy, B. Palakshi
author_sort Loh, Wan-Sin
collection PubMed
description In the title compound, C(31)H(24)Br(4)N(2)O, one of the bromo­phenyl rings is disordered over two orientations with occupancies of 0.69 (2) and 0.31 (2). The bicyclo­[3.3.1]nonane ring system adopts a chair–boat conformation. In the crystal structure, mol­ecules are linked into chains along the c axis by inter­molecular C—H⋯O and N—H⋯O hydrogen bonds. Further stabilization is provided by C—H⋯π inter­actions.
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spelling pubmed-29798662010-12-30 2,4,6,8-Tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one Loh, Wan-Sin Fun, Hoong-Kun Sarveswari, S. Vijayakumar, V. Reddy, B. Palakshi Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(31)H(24)Br(4)N(2)O, one of the bromo­phenyl rings is disordered over two orientations with occupancies of 0.69 (2) and 0.31 (2). The bicyclo­[3.3.1]nonane ring system adopts a chair–boat conformation. In the crystal structure, mol­ecules are linked into chains along the c axis by inter­molecular C—H⋯O and N—H⋯O hydrogen bonds. Further stabilization is provided by C—H⋯π inter­actions. International Union of Crystallography 2010-01-09 /pmc/articles/PMC2979866/ /pubmed/21579706 http://dx.doi.org/10.1107/S1600536809055226 Text en © Loh et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Loh, Wan-Sin
Fun, Hoong-Kun
Sarveswari, S.
Vijayakumar, V.
Reddy, B. Palakshi
2,4,6,8-Tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one
title 2,4,6,8-Tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one
title_full 2,4,6,8-Tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one
title_fullStr 2,4,6,8-Tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one
title_full_unstemmed 2,4,6,8-Tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one
title_short 2,4,6,8-Tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one
title_sort 2,4,6,8-tetra­kis(4-bromo­phen­yl)-3,7-diaza­bicyclo­[3.3.1]nonan-9-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979866/
https://www.ncbi.nlm.nih.gov/pubmed/21579706
http://dx.doi.org/10.1107/S1600536809055226
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