Bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate

The title compound, C(28)H(20)N(2)O(8), was synthesized by the reaction of isobenzofuran-1,3-dione and 2-amino­ethanol in a one-pot reaction. The benzene and five-membered rings are slightly twisted to each other, making dihedral angles of 2.77 (9) and 1.77 (10)°. The rings of the phthalimide groups...

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Detalles Bibliográficos
Autores principales: Yang, Kai, Guo, Qiang, Wang, Shi-Fan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979961/
https://www.ncbi.nlm.nih.gov/pubmed/21579766
http://dx.doi.org/10.1107/S160053680905524X
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author Yang, Kai
Guo, Qiang
Wang, Shi-Fan
author_facet Yang, Kai
Guo, Qiang
Wang, Shi-Fan
author_sort Yang, Kai
collection PubMed
description The title compound, C(28)H(20)N(2)O(8), was synthesized by the reaction of isobenzofuran-1,3-dione and 2-amino­ethanol in a one-pot reaction. The benzene and five-membered rings are slightly twisted to each other, making dihedral angles of 2.77 (9) and 1.77 (10)°. The rings of the phthalimide groups make dihedral angle of 57.64 (7) and 83.46 (7)° with the central benzene ring. Weak C—H⋯O, C—H⋯π and π–π [centroid–centroid distance = 3.446 (1) and 3.599 (1) Å] inter­actions reinforce the cohesion of the crystal.
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spelling pubmed-29799612010-12-30 Bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate Yang, Kai Guo, Qiang Wang, Shi-Fan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(28)H(20)N(2)O(8), was synthesized by the reaction of isobenzofuran-1,3-dione and 2-amino­ethanol in a one-pot reaction. The benzene and five-membered rings are slightly twisted to each other, making dihedral angles of 2.77 (9) and 1.77 (10)°. The rings of the phthalimide groups make dihedral angle of 57.64 (7) and 83.46 (7)° with the central benzene ring. Weak C—H⋯O, C—H⋯π and π–π [centroid–centroid distance = 3.446 (1) and 3.599 (1) Å] inter­actions reinforce the cohesion of the crystal. International Union of Crystallography 2010-01-13 /pmc/articles/PMC2979961/ /pubmed/21579766 http://dx.doi.org/10.1107/S160053680905524X Text en © Yang et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yang, Kai
Guo, Qiang
Wang, Shi-Fan
Bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate
title Bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate
title_full Bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate
title_fullStr Bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate
title_full_unstemmed Bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate
title_short Bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate
title_sort bis[2-(1,3-dioxoisoindolin-2-yl)eth­yl] phthalate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979961/
https://www.ncbi.nlm.nih.gov/pubmed/21579766
http://dx.doi.org/10.1107/S160053680905524X
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AT guoqiang bis213dioxoisoindolin2ylethylphthalate
AT wangshifan bis213dioxoisoindolin2ylethylphthalate

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