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12-Ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate
The title compound, C(23)H(23)NO(5)·CH(2)Cl(2), was obtained via the alkylation of the 12-hydroxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine salt. The benzo[c]phenanthridine ring system is essentially planar, with a mean out-of-plane deviation of 0.026 Å. A dicloromethane molecule of solvation...
| Autores principales: | , , , , |
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| Formato: | Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2009
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| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980059/ https://www.ncbi.nlm.nih.gov/pubmed/21580014 http://dx.doi.org/10.1107/S1600536809050818 |
| _version_ | 1782191567613722624 |
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| author | Ronaldson, Michael Maheux, Chad R. Nyangulu, James M. Cameron, T. Stanley Aquino, Manuel A.S. |
| author_facet | Ronaldson, Michael Maheux, Chad R. Nyangulu, James M. Cameron, T. Stanley Aquino, Manuel A.S. |
| author_sort | Ronaldson, Michael |
| collection | PubMed |
| description | The title compound, C(23)H(23)NO(5)·CH(2)Cl(2), was obtained via the alkylation of the 12-hydroxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine salt. The benzo[c]phenanthridine ring system is essentially planar, with a mean out-of-plane deviation of 0.026 Å. A dicloromethane molecule of solvation is present and located between the sheets of phenanthridine molecules, preventing any significant intermolecular hydrogen-bonding or π–π interactions. |
| format | Text |
| id | pubmed-2980059 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2009 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-29800592010-12-30 12-Ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate Ronaldson, Michael Maheux, Chad R. Nyangulu, James M. Cameron, T. Stanley Aquino, Manuel A.S. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(23)H(23)NO(5)·CH(2)Cl(2), was obtained via the alkylation of the 12-hydroxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine salt. The benzo[c]phenanthridine ring system is essentially planar, with a mean out-of-plane deviation of 0.026 Å. A dicloromethane molecule of solvation is present and located between the sheets of phenanthridine molecules, preventing any significant intermolecular hydrogen-bonding or π–π interactions. International Union of Crystallography 2009-12-12 /pmc/articles/PMC2980059/ /pubmed/21580014 http://dx.doi.org/10.1107/S1600536809050818 Text en © Ronaldson et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Ronaldson, Michael Maheux, Chad R. Nyangulu, James M. Cameron, T. Stanley Aquino, Manuel A.S. 12-Ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate |
| title | 12-Ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate |
| title_full | 12-Ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate |
| title_fullStr | 12-Ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate |
| title_full_unstemmed | 12-Ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate |
| title_short | 12-Ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate |
| title_sort | 12-ethoxy-2,3,8,9-tetramethoxybenzo[c]phenanthridine dichloromethane solvate |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980059/ https://www.ncbi.nlm.nih.gov/pubmed/21580014 http://dx.doi.org/10.1107/S1600536809050818 |
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