N-(2,4,5-Trichloro­phen­yl)maleamic acid

The title compound, C(10)H(6)Cl(3)NO(3), crystallizes with two independent mol­ecules in the asymmetric unit. The mol­ecular structure is stabilized by a short intra­molecular O—H⋯O hydrogen bond within the maleamic unit. In the crystal, each mol­ecule self-associates via N—H⋯O hydrogen bonds into c...

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Detalles Bibliográficos
Autores principales: Gowda, B. Thimme, Tokarčík, Miroslav, Kožíšek, Jozef, Shakuntala, K., Fuess, Hartmut
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980077/
https://www.ncbi.nlm.nih.gov/pubmed/21580067
http://dx.doi.org/10.1107/S1600536809052520
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author Gowda, B. Thimme
Tokarčík, Miroslav
Kožíšek, Jozef
Shakuntala, K.
Fuess, Hartmut
author_facet Gowda, B. Thimme
Tokarčík, Miroslav
Kožíšek, Jozef
Shakuntala, K.
Fuess, Hartmut
author_sort Gowda, B. Thimme
collection PubMed
description The title compound, C(10)H(6)Cl(3)NO(3), crystallizes with two independent mol­ecules in the asymmetric unit. The mol­ecular structure is stabilized by a short intra­molecular O—H⋯O hydrogen bond within the maleamic unit. In the crystal, each mol­ecule self-associates via N—H⋯O hydrogen bonds into chains, each running along the b axis. Two short inter­molecular Cl⋯O contacts [3.1267 (15) and 3.0523 (12) Å] and C—H⋯O inter­actions inter­connect these chains into a three-dimensional network.
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spelling pubmed-29800772010-12-30 N-(2,4,5-Trichloro­phen­yl)maleamic acid Gowda, B. Thimme Tokarčík, Miroslav Kožíšek, Jozef Shakuntala, K. Fuess, Hartmut Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(6)Cl(3)NO(3), crystallizes with two independent mol­ecules in the asymmetric unit. The mol­ecular structure is stabilized by a short intra­molecular O—H⋯O hydrogen bond within the maleamic unit. In the crystal, each mol­ecule self-associates via N—H⋯O hydrogen bonds into chains, each running along the b axis. Two short inter­molecular Cl⋯O contacts [3.1267 (15) and 3.0523 (12) Å] and C—H⋯O inter­actions inter­connect these chains into a three-dimensional network. International Union of Crystallography 2009-12-16 /pmc/articles/PMC2980077/ /pubmed/21580067 http://dx.doi.org/10.1107/S1600536809052520 Text en © Gowda et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gowda, B. Thimme
Tokarčík, Miroslav
Kožíšek, Jozef
Shakuntala, K.
Fuess, Hartmut
N-(2,4,5-Trichloro­phen­yl)maleamic acid
title N-(2,4,5-Trichloro­phen­yl)maleamic acid
title_full N-(2,4,5-Trichloro­phen­yl)maleamic acid
title_fullStr N-(2,4,5-Trichloro­phen­yl)maleamic acid
title_full_unstemmed N-(2,4,5-Trichloro­phen­yl)maleamic acid
title_short N-(2,4,5-Trichloro­phen­yl)maleamic acid
title_sort n-(2,4,5-trichloro­phen­yl)maleamic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980077/
https://www.ncbi.nlm.nih.gov/pubmed/21580067
http://dx.doi.org/10.1107/S1600536809052520
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AT tokarcikmiroslav n245trichlorophenylmaleamicacid
AT kozisekjozef n245trichlorophenylmaleamicacid
AT shakuntalak n245trichlorophenylmaleamicacid
AT fuesshartmut n245trichlorophenylmaleamicacid

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