(E)-N′-(3,4,5-Trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate

In the title compound, C(21)H(21)N(3)O(5)·CH(4)O, the quinoline plane and the benzene ring form a dihedral angle of 3.6 (2)°. The methanol solvent mol­ecule is linked with the acetohydrazide mol­ecule via O—H⋯N and N—H⋯O hydrogen bonds. In the crystal structure, weak inter­molecular C—H⋯O hydrogen b...

Descripción completa

Detalles Bibliográficos
Autor principal: Zeng, Ling
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980132/
https://www.ncbi.nlm.nih.gov/pubmed/21580111
http://dx.doi.org/10.1107/S1600536809051113
_version_ 1782191585113407488
author Zeng, Ling
author_facet Zeng, Ling
author_sort Zeng, Ling
collection PubMed
description In the title compound, C(21)H(21)N(3)O(5)·CH(4)O, the quinoline plane and the benzene ring form a dihedral angle of 3.6 (2)°. The methanol solvent mol­ecule is linked with the acetohydrazide mol­ecule via O—H⋯N and N—H⋯O hydrogen bonds. In the crystal structure, weak inter­molecular C—H⋯O hydrogen bonds help to consolidate the crystal packing, which also exhibits π–π inter­actions, as indicated by short distances of 3.739 (4) Å between the centroids of the aromatic rings.
format Text
id pubmed-2980132
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29801322010-12-30 (E)-N′-(3,4,5-Trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate Zeng, Ling Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(21)H(21)N(3)O(5)·CH(4)O, the quinoline plane and the benzene ring form a dihedral angle of 3.6 (2)°. The methanol solvent mol­ecule is linked with the acetohydrazide mol­ecule via O—H⋯N and N—H⋯O hydrogen bonds. In the crystal structure, weak inter­molecular C—H⋯O hydrogen bonds help to consolidate the crystal packing, which also exhibits π–π inter­actions, as indicated by short distances of 3.739 (4) Å between the centroids of the aromatic rings. International Union of Crystallography 2009-12-04 /pmc/articles/PMC2980132/ /pubmed/21580111 http://dx.doi.org/10.1107/S1600536809051113 Text en © Ling Zeng 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zeng, Ling
(E)-N′-(3,4,5-Trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate
title (E)-N′-(3,4,5-Trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate
title_full (E)-N′-(3,4,5-Trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate
title_fullStr (E)-N′-(3,4,5-Trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate
title_full_unstemmed (E)-N′-(3,4,5-Trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate
title_short (E)-N′-(3,4,5-Trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate
title_sort (e)-n′-(3,4,5-trimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980132/
https://www.ncbi.nlm.nih.gov/pubmed/21580111
http://dx.doi.org/10.1107/S1600536809051113
work_keys_str_mv AT zengling en345trimethoxybenzylidene28quinolyloxyacetohydrazidemethanolsolvate

Ejemplares similares