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(E)-4-(2-Chlorobenzylideneamino)-3-(2-chlorophenyl)-1H-1,2,4-triazole-5(4H)-thione–(E)-1,5-bis(2-chlorobenzylidene)thiocarbonohydrazide–methanol (1/1/1)
In the title compound, C(15)H(12)Cl(2)N(4)S·C(15)H(10)Cl(2)N(4)S·C(2)H(6)O, the two chlorophenyl rings of the triazole derivative form dihedral angles of 65.7 (2) and 44.2 (2)° with the triazole ring. In the thiocarbonohydrazide derivative, the dihedral angle between the two chlorophenyl rings is...
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980177/ https://www.ncbi.nlm.nih.gov/pubmed/21580033 http://dx.doi.org/10.1107/S1600536809053203 |
Sumario: | In the title compound, C(15)H(12)Cl(2)N(4)S·C(15)H(10)Cl(2)N(4)S·C(2)H(6)O, the two chlorophenyl rings of the triazole derivative form dihedral angles of 65.7 (2) and 44.2 (2)° with the triazole ring. In the thiocarbonohydrazide derivative, the dihedral angle between the two chlorophenyl rings is 5.4 (2)°. In the crystal, the triazole, thiocarbonohydrazide and methanol molecules are linked by N—H⋯O, N—H⋯S and O—H⋯S hydrogen bonds, forming a hexameric unit. |
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