N-(3,4-Dichloro­phen­yl)-3-oxo­butanamide

In the title compound. C(10)H(9)Cl(2)NO(2), the acetamide residue is twisted out of the phenyl ring plane by 25.40 (9)°. An intra­molecular C—H⋯O close contact is observed. The N atom of the butanamide unit forms an inter­molecular N—H⋯O hydrogen bond with the symmetry-related carbonyl O atom, inter...

Descripción completa

Detalles Bibliográficos
Autores principales: Jotani, Mukesh M., Jasinski, Jerry P., Baldaniya, Bharat B., Butcher, Ray J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980202/
https://www.ncbi.nlm.nih.gov/pubmed/21580160
http://dx.doi.org/10.1107/S1600536809051307
_version_ 1782191602141233152
author Jotani, Mukesh M.
Jasinski, Jerry P.
Baldaniya, Bharat B.
Butcher, Ray J.
author_facet Jotani, Mukesh M.
Jasinski, Jerry P.
Baldaniya, Bharat B.
Butcher, Ray J.
author_sort Jotani, Mukesh M.
collection PubMed
description In the title compound. C(10)H(9)Cl(2)NO(2), the acetamide residue is twisted out of the phenyl ring plane by 25.40 (9)°. An intra­molecular C—H⋯O close contact is observed. The N atom of the butanamide unit forms an inter­molecular N—H⋯O hydrogen bond with the symmetry-related carbonyl O atom, inter­linking mol­ecules into a C(4) chain along [100]. Additional C—H⋯O inter­molecular inter­actions and Cl⋯Cl contacts [3.4364 (8) Å] contribute to the stability of the crystal packing.
format Text
id pubmed-2980202
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29802022010-12-30 N-(3,4-Dichloro­phen­yl)-3-oxo­butanamide Jotani, Mukesh M. Jasinski, Jerry P. Baldaniya, Bharat B. Butcher, Ray J. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound. C(10)H(9)Cl(2)NO(2), the acetamide residue is twisted out of the phenyl ring plane by 25.40 (9)°. An intra­molecular C—H⋯O close contact is observed. The N atom of the butanamide unit forms an inter­molecular N—H⋯O hydrogen bond with the symmetry-related carbonyl O atom, inter­linking mol­ecules into a C(4) chain along [100]. Additional C—H⋯O inter­molecular inter­actions and Cl⋯Cl contacts [3.4364 (8) Å] contribute to the stability of the crystal packing. International Union of Crystallography 2009-12-04 /pmc/articles/PMC2980202/ /pubmed/21580160 http://dx.doi.org/10.1107/S1600536809051307 Text en © Jotani et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jotani, Mukesh M.
Jasinski, Jerry P.
Baldaniya, Bharat B.
Butcher, Ray J.
N-(3,4-Dichloro­phen­yl)-3-oxo­butanamide
title N-(3,4-Dichloro­phen­yl)-3-oxo­butanamide
title_full N-(3,4-Dichloro­phen­yl)-3-oxo­butanamide
title_fullStr N-(3,4-Dichloro­phen­yl)-3-oxo­butanamide
title_full_unstemmed N-(3,4-Dichloro­phen­yl)-3-oxo­butanamide
title_short N-(3,4-Dichloro­phen­yl)-3-oxo­butanamide
title_sort n-(3,4-dichloro­phen­yl)-3-oxo­butanamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980202/
https://www.ncbi.nlm.nih.gov/pubmed/21580160
http://dx.doi.org/10.1107/S1600536809051307
work_keys_str_mv AT jotanimukeshm n34dichlorophenyl3oxobutanamide
AT jasinskijerryp n34dichlorophenyl3oxobutanamide
AT baldaniyabharatb n34dichlorophenyl3oxobutanamide
AT butcherrayj n34dichlorophenyl3oxobutanamide

Ejemplares similares