N,N′-Bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate

The title compound, C(24)H(16)Br(2)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are twisted away from the naphthalene ring system by 62.67 (8) and 75.93 (7)°. The crystal packing is stabilized by N—H⋯O and C—H⋯O hydrogen bonds. Each of the dimethyl­acetamide so...

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Autor principal: Jing, Lin-Hai
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980233/
https://www.ncbi.nlm.nih.gov/pubmed/21580134
http://dx.doi.org/10.1107/S1600536809051447
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author Jing, Lin-Hai
author_facet Jing, Lin-Hai
author_sort Jing, Lin-Hai
collection PubMed
description The title compound, C(24)H(16)Br(2)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are twisted away from the naphthalene ring system by 62.67 (8) and 75.93 (7)°. The crystal packing is stabilized by N—H⋯O and C—H⋯O hydrogen bonds. Each of the dimethyl­acetamide solvent mol­ecules is disordered over two positions, with occupancy ratios of 0.556 (7):0.444 (7) and 0.654 (7):0.346 (7).
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spelling pubmed-29802332010-12-30 N,N′-Bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate Jing, Lin-Hai Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(24)H(16)Br(2)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are twisted away from the naphthalene ring system by 62.67 (8) and 75.93 (7)°. The crystal packing is stabilized by N—H⋯O and C—H⋯O hydrogen bonds. Each of the dimethyl­acetamide solvent mol­ecules is disordered over two positions, with occupancy ratios of 0.556 (7):0.444 (7) and 0.654 (7):0.346 (7). International Union of Crystallography 2009-12-04 /pmc/articles/PMC2980233/ /pubmed/21580134 http://dx.doi.org/10.1107/S1600536809051447 Text en © Lin-Hai Jing 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jing, Lin-Hai
N,N′-Bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title N,N′-Bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_full N,N′-Bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_fullStr N,N′-Bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_full_unstemmed N,N′-Bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_short N,N′-Bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_sort n,n′-bis(4-bromo­phen­yl)naphthalene-1,4-dicarboxamide n,n-dimethyl­acetamide disolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980233/
https://www.ncbi.nlm.nih.gov/pubmed/21580134
http://dx.doi.org/10.1107/S1600536809051447
work_keys_str_mv AT jinglinhai nnbis4bromophenylnaphthalene14dicarboxamidenndimethylacetamidedisolvate

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