12-(2-Methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12H-benzo[a]xanthen-11(10H)-one

The title compound, C(26)H(24)O(3), was synthesized via the coupling of 2-methoxy­benzaldehyde, 2-naphthol and 5,5-dimethyl­cyclo­hexane-1,3-dione. The pyran ring adopts a boat conformation, while the cyclo­hexenone ring is in an envelope conformation. The 2-methoxy­phenyl ring is almost perpendic­u...

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Detalles Bibliográficos
Autores principales: Li, De-Ling, Wang, Li-Hong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980265/
https://www.ncbi.nlm.nih.gov/pubmed/21580008
http://dx.doi.org/10.1107/S1600536809052210
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author Li, De-Ling
Wang, Li-Hong
author_facet Li, De-Ling
Wang, Li-Hong
author_sort Li, De-Ling
collection PubMed
description The title compound, C(26)H(24)O(3), was synthesized via the coupling of 2-methoxy­benzaldehyde, 2-naphthol and 5,5-dimethyl­cyclo­hexane-1,3-dione. The pyran ring adopts a boat conformation, while the cyclo­hexenone ring is in an envelope conformation. The 2-methoxy­phenyl ring is almost perpendic­ular to the plane through the four C atoms of the pyran ring [dihedral angle = 88.76 (9)°].
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spelling pubmed-29802652010-12-30 12-(2-Methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12H-benzo[a]xanthen-11(10H)-one Li, De-Ling Wang, Li-Hong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(26)H(24)O(3), was synthesized via the coupling of 2-methoxy­benzaldehyde, 2-naphthol and 5,5-dimethyl­cyclo­hexane-1,3-dione. The pyran ring adopts a boat conformation, while the cyclo­hexenone ring is in an envelope conformation. The 2-methoxy­phenyl ring is almost perpendic­ular to the plane through the four C atoms of the pyran ring [dihedral angle = 88.76 (9)°]. International Union of Crystallography 2009-12-12 /pmc/articles/PMC2980265/ /pubmed/21580008 http://dx.doi.org/10.1107/S1600536809052210 Text en © Li and Wang 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, De-Ling
Wang, Li-Hong
12-(2-Methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12H-benzo[a]xanthen-11(10H)-one
title 12-(2-Methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12H-benzo[a]xanthen-11(10H)-one
title_full 12-(2-Methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12H-benzo[a]xanthen-11(10H)-one
title_fullStr 12-(2-Methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12H-benzo[a]xanthen-11(10H)-one
title_full_unstemmed 12-(2-Methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12H-benzo[a]xanthen-11(10H)-one
title_short 12-(2-Methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12H-benzo[a]xanthen-11(10H)-one
title_sort 12-(2-methoxyphenyl)-9,9-dimethyl-8,9-dihydro-12h-benzo[a]xanthen-11(10h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2980265/
https://www.ncbi.nlm.nih.gov/pubmed/21580008
http://dx.doi.org/10.1107/S1600536809052210
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AT wanglihong 122methoxyphenyl99dimethyl89dihydro12hbenzoaxanthen1110hone

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