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1-(3,4-Dimethylbenzylidene)-4-ethylthiosemicarbazide
The title compound, C(12)H(17)N(3)S, was prepared by the reaction of 4-ethylthiosemicarbazide and 3,4-dimethylbenzaldehyde. The dihedral angle between the thiourea unit and the benzene ring is 7.09 (8)°. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds occur.
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2010
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983114/ https://www.ncbi.nlm.nih.gov/pubmed/21587653 http://dx.doi.org/10.1107/S1600536810038389 |
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author | Li, Yu-Feng Meng, Fan-Yong |
author_facet | Li, Yu-Feng Meng, Fan-Yong |
author_sort | Li, Yu-Feng |
collection | PubMed |
description | The title compound, C(12)H(17)N(3)S, was prepared by the reaction of 4-ethylthiosemicarbazide and 3,4-dimethylbenzaldehyde. The dihedral angle between the thiourea unit and the benzene ring is 7.09 (8)°. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds occur. |
format | Text |
id | pubmed-2983114 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2010 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29831142010-12-30 1-(3,4-Dimethylbenzylidene)-4-ethylthiosemicarbazide Li, Yu-Feng Meng, Fan-Yong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(12)H(17)N(3)S, was prepared by the reaction of 4-ethylthiosemicarbazide and 3,4-dimethylbenzaldehyde. The dihedral angle between the thiourea unit and the benzene ring is 7.09 (8)°. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds occur. International Union of Crystallography 2010-09-30 /pmc/articles/PMC2983114/ /pubmed/21587653 http://dx.doi.org/10.1107/S1600536810038389 Text en © Li and Meng 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Li, Yu-Feng Meng, Fan-Yong 1-(3,4-Dimethylbenzylidene)-4-ethylthiosemicarbazide |
title | 1-(3,4-Dimethylbenzylidene)-4-ethylthiosemicarbazide |
title_full | 1-(3,4-Dimethylbenzylidene)-4-ethylthiosemicarbazide |
title_fullStr | 1-(3,4-Dimethylbenzylidene)-4-ethylthiosemicarbazide |
title_full_unstemmed | 1-(3,4-Dimethylbenzylidene)-4-ethylthiosemicarbazide |
title_short | 1-(3,4-Dimethylbenzylidene)-4-ethylthiosemicarbazide |
title_sort | 1-(3,4-dimethylbenzylidene)-4-ethylthiosemicarbazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983114/ https://www.ncbi.nlm.nih.gov/pubmed/21587653 http://dx.doi.org/10.1107/S1600536810038389 |
work_keys_str_mv | AT liyufeng 134dimethylbenzylidene4ethylthiosemicarbazide AT mengfanyong 134dimethylbenzylidene4ethylthiosemicarbazide |