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1-(3,4-Dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide

The title compound, C(12)H(17)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and 3,4-dimethyl­benzaldehyde. The dihedral angle between the thiourea unit and the benzene ring is 7.09 (8)°. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds occur.

Detalles Bibliográficos
Autores principales: Li, Yu-Feng, Meng, Fan-Yong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983114/
https://www.ncbi.nlm.nih.gov/pubmed/21587653
http://dx.doi.org/10.1107/S1600536810038389
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author Li, Yu-Feng
Meng, Fan-Yong
author_facet Li, Yu-Feng
Meng, Fan-Yong
author_sort Li, Yu-Feng
collection PubMed
description The title compound, C(12)H(17)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and 3,4-dimethyl­benzaldehyde. The dihedral angle between the thiourea unit and the benzene ring is 7.09 (8)°. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds occur.
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spelling pubmed-29831142010-12-30 1-(3,4-Dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide Li, Yu-Feng Meng, Fan-Yong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(12)H(17)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and 3,4-dimethyl­benzaldehyde. The dihedral angle between the thiourea unit and the benzene ring is 7.09 (8)°. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds occur. International Union of Crystallography 2010-09-30 /pmc/articles/PMC2983114/ /pubmed/21587653 http://dx.doi.org/10.1107/S1600536810038389 Text en © Li and Meng 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Yu-Feng
Meng, Fan-Yong
1-(3,4-Dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide
title 1-(3,4-Dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide
title_full 1-(3,4-Dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide
title_fullStr 1-(3,4-Dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide
title_full_unstemmed 1-(3,4-Dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide
title_short 1-(3,4-Dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide
title_sort 1-(3,4-dimethyl­benzyl­idene)-4-ethyl­thio­semicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983114/
https://www.ncbi.nlm.nih.gov/pubmed/21587653
http://dx.doi.org/10.1107/S1600536810038389
work_keys_str_mv AT liyufeng 134dimethylbenzylidene4ethylthiosemicarbazide
AT mengfanyong 134dimethylbenzylidene4ethylthiosemicarbazide