N′-(3,5-Dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate

In the title compound, C(14)H(9)Cl(2)N(3)O(4)·CH(4)O, the dihedral angle between the two benzene rings in the hydrazone mol­ecule is 6.3 (3)°. An intra­molecular N—H⋯O hydrogen bond stabilizes the mol­ecular conformation. In the crystal, centrosymmetrically related mol­ecules are linked through inte...

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Autor principal: Zhu, Hai-Yun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983133/
https://www.ncbi.nlm.nih.gov/pubmed/21587548
http://dx.doi.org/10.1107/S1600536810036184
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author Zhu, Hai-Yun
author_facet Zhu, Hai-Yun
author_sort Zhu, Hai-Yun
collection PubMed
description In the title compound, C(14)H(9)Cl(2)N(3)O(4)·CH(4)O, the dihedral angle between the two benzene rings in the hydrazone mol­ecule is 6.3 (3)°. An intra­molecular N—H⋯O hydrogen bond stabilizes the mol­ecular conformation. In the crystal, centrosymmetrically related mol­ecules are linked through inter­molecular O—H⋯O and N—H⋯O hydrogen bonds.
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spelling pubmed-29831332010-12-30 N′-(3,5-Dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate Zhu, Hai-Yun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(9)Cl(2)N(3)O(4)·CH(4)O, the dihedral angle between the two benzene rings in the hydrazone mol­ecule is 6.3 (3)°. An intra­molecular N—H⋯O hydrogen bond stabilizes the mol­ecular conformation. In the crystal, centrosymmetrically related mol­ecules are linked through inter­molecular O—H⋯O and N—H⋯O hydrogen bonds. International Union of Crystallography 2010-09-15 /pmc/articles/PMC2983133/ /pubmed/21587548 http://dx.doi.org/10.1107/S1600536810036184 Text en © Hai-Yun Zhu 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhu, Hai-Yun
N′-(3,5-Dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate
title N′-(3,5-Dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate
title_full N′-(3,5-Dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate
title_fullStr N′-(3,5-Dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate
title_full_unstemmed N′-(3,5-Dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate
title_short N′-(3,5-Dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate
title_sort n′-(3,5-dichloro-2-hy­droxy­benzyl­idene)-4-nitro­benzohydrazide methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983133/
https://www.ncbi.nlm.nih.gov/pubmed/21587548
http://dx.doi.org/10.1107/S1600536810036184
work_keys_str_mv AT zhuhaiyun n35dichloro2hydroxybenzylidene4nitrobenzohydrazidemethanolsolvate

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