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4,4′-Dichloro-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol
Molecules of the the title compound, C(21)H(24)Cl(2)N(2)O(2), are located on a twofold rotation axis, which passes through the C atom linking the two N atoms. Two intramolecular O—H⋯N hydrogen bonds were observed. In the crystal, non-classical intermolecular C—H⋯O hydrogen bonds link the molecul...
| Autores principales: | , , , , |
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| Formato: | Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2010
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| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983180/ https://www.ncbi.nlm.nih.gov/pubmed/21587614 http://dx.doi.org/10.1107/S160053681003792X |
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| author | Rivera, Augusto Quiroga, Diego Ríos-Motta, Jaime Dušek, Michal Fejfarová, Karla |
| author_facet | Rivera, Augusto Quiroga, Diego Ríos-Motta, Jaime Dušek, Michal Fejfarová, Karla |
| author_sort | Rivera, Augusto |
| collection | PubMed |
| description | Molecules of the the title compound, C(21)H(24)Cl(2)N(2)O(2), are located on a twofold rotation axis, which passes through the C atom linking the two N atoms. Two intramolecular O—H⋯N hydrogen bonds were observed. In the crystal, non-classical intermolecular C—H⋯O hydrogen bonds link the molecules into chains along the a axis. The crystal studied was a racemic twin. |
| format | Text |
| id | pubmed-2983180 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2010 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-29831802010-12-30 4,4′-Dichloro-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol Rivera, Augusto Quiroga, Diego Ríos-Motta, Jaime Dušek, Michal Fejfarová, Karla Acta Crystallogr Sect E Struct Rep Online Organic Papers Molecules of the the title compound, C(21)H(24)Cl(2)N(2)O(2), are located on a twofold rotation axis, which passes through the C atom linking the two N atoms. Two intramolecular O—H⋯N hydrogen bonds were observed. In the crystal, non-classical intermolecular C—H⋯O hydrogen bonds link the molecules into chains along the a axis. The crystal studied was a racemic twin. International Union of Crystallography 2010-09-30 /pmc/articles/PMC2983180/ /pubmed/21587614 http://dx.doi.org/10.1107/S160053681003792X Text en © Rivera et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Rivera, Augusto Quiroga, Diego Ríos-Motta, Jaime Dušek, Michal Fejfarová, Karla 4,4′-Dichloro-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol |
| title | 4,4′-Dichloro-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol |
| title_full | 4,4′-Dichloro-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol |
| title_fullStr | 4,4′-Dichloro-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol |
| title_full_unstemmed | 4,4′-Dichloro-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol |
| title_short | 4,4′-Dichloro-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol |
| title_sort | 4,4′-dichloro-2,2′-[(3ar,7ar/3as,7as)-2,3,3a,4,5,6,7,7a-octahydro-1h-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983180/ https://www.ncbi.nlm.nih.gov/pubmed/21587614 http://dx.doi.org/10.1107/S160053681003792X |
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