1-(2,4-Dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide

The title compound, C(10)H(11)Cl(2)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and 2,4-dichloro­benzaldehyde. It is approximately planar, the dihedral angle between the benzene ring and the thio­urea unit being 8.43 (18)°. In the crystal, inversion dimers linked by pairs of N—H...

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Detalles Bibliográficos
Autor principal: Li, Yu-Feng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983246/
https://www.ncbi.nlm.nih.gov/pubmed/21587538
http://dx.doi.org/10.1107/S1600536810035671
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author Li, Yu-Feng
author_facet Li, Yu-Feng
author_sort Li, Yu-Feng
collection PubMed
description The title compound, C(10)H(11)Cl(2)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and 2,4-dichloro­benzaldehyde. It is approximately planar, the dihedral angle between the benzene ring and the thio­urea unit being 8.43 (18)°. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops.
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spelling pubmed-29832462010-12-30 1-(2,4-Dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide Li, Yu-Feng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(11)Cl(2)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and 2,4-dichloro­benzaldehyde. It is approximately planar, the dihedral angle between the benzene ring and the thio­urea unit being 8.43 (18)°. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops. International Union of Crystallography 2010-09-11 /pmc/articles/PMC2983246/ /pubmed/21587538 http://dx.doi.org/10.1107/S1600536810035671 Text en © Yu-Feng Li 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Yu-Feng
1-(2,4-Dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide
title 1-(2,4-Dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide
title_full 1-(2,4-Dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide
title_fullStr 1-(2,4-Dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide
title_full_unstemmed 1-(2,4-Dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide
title_short 1-(2,4-Dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide
title_sort 1-(2,4-dichloro­benzyl­idene)-4-ethyl­thio­semicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983246/
https://www.ncbi.nlm.nih.gov/pubmed/21587538
http://dx.doi.org/10.1107/S1600536810035671
work_keys_str_mv AT liyufeng 124dichlorobenzylidene4ethylthiosemicarbazide

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