Cargando…

2-Dibutyl­amino-1-(2,7-dichloro-9H-fluoren-4-yl)ethanol

In the title compound, C(23)H(29)Cl(2)NO, the fluorene ring is essentially planar, with a maximum deviation from the mean plane of 0.041 (1) Å. The amine group adopts a pyramidal configuration, the sum of the bond angles being 336.2 (3)°. In the crystal, the mol­ecules are linked into dimers by inte...

Descripción completa

Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Yeap, Chin Sing, Vijesh, A. M., Isloor, Arun M, Vasudeva, P. K.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983289/
https://www.ncbi.nlm.nih.gov/pubmed/21587598
http://dx.doi.org/10.1107/S1600536810037566
_version_ 1782191845982339072
author Fun, Hoong-Kun
Yeap, Chin Sing
Vijesh, A. M.
Isloor, Arun M
Vasudeva, P. K.
author_facet Fun, Hoong-Kun
Yeap, Chin Sing
Vijesh, A. M.
Isloor, Arun M
Vasudeva, P. K.
author_sort Fun, Hoong-Kun
collection PubMed
description In the title compound, C(23)H(29)Cl(2)NO, the fluorene ring is essentially planar, with a maximum deviation from the mean plane of 0.041 (1) Å. The amine group adopts a pyramidal configuration, the sum of the bond angles being 336.2 (3)°. In the crystal, the mol­ecules are linked into dimers by inter­molecular O—H⋯N and C—H⋯O hydrogen bonds. Weak C—H⋯π and π–π [centroid–centroid distance = 3.7544 (7) Å] inter­actions are also observed.
format Text
id pubmed-2983289
institution National Center for Biotechnology Information
language English
publishDate 2010
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29832892010-12-30 2-Dibutyl­amino-1-(2,7-dichloro-9H-fluoren-4-yl)ethanol Fun, Hoong-Kun Yeap, Chin Sing Vijesh, A. M. Isloor, Arun M Vasudeva, P. K. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(23)H(29)Cl(2)NO, the fluorene ring is essentially planar, with a maximum deviation from the mean plane of 0.041 (1) Å. The amine group adopts a pyramidal configuration, the sum of the bond angles being 336.2 (3)°. In the crystal, the mol­ecules are linked into dimers by inter­molecular O—H⋯N and C—H⋯O hydrogen bonds. Weak C—H⋯π and π–π [centroid–centroid distance = 3.7544 (7) Å] inter­actions are also observed. International Union of Crystallography 2010-09-25 /pmc/articles/PMC2983289/ /pubmed/21587598 http://dx.doi.org/10.1107/S1600536810037566 Text en © Fun et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Yeap, Chin Sing
Vijesh, A. M.
Isloor, Arun M
Vasudeva, P. K.
2-Dibutyl­amino-1-(2,7-dichloro-9H-fluoren-4-yl)ethanol
title 2-Dibutyl­amino-1-(2,7-dichloro-9H-fluoren-4-yl)ethanol
title_full 2-Dibutyl­amino-1-(2,7-dichloro-9H-fluoren-4-yl)ethanol
title_fullStr 2-Dibutyl­amino-1-(2,7-dichloro-9H-fluoren-4-yl)ethanol
title_full_unstemmed 2-Dibutyl­amino-1-(2,7-dichloro-9H-fluoren-4-yl)ethanol
title_short 2-Dibutyl­amino-1-(2,7-dichloro-9H-fluoren-4-yl)ethanol
title_sort 2-dibutyl­amino-1-(2,7-dichloro-9h-fluoren-4-yl)ethanol
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983289/
https://www.ncbi.nlm.nih.gov/pubmed/21587598
http://dx.doi.org/10.1107/S1600536810037566
work_keys_str_mv AT funhoongkun 2dibutylamino127dichloro9hfluoren4ylethanol
AT yeapchinsing 2dibutylamino127dichloro9hfluoren4ylethanol
AT vijesham 2dibutylamino127dichloro9hfluoren4ylethanol
AT isloorarunm 2dibutylamino127dichloro9hfluoren4ylethanol
AT vasudevapk 2dibutylamino127dichloro9hfluoren4ylethanol