Ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate

In the title compound, C(15)H(12)ClF(3)N(4)O(2), the dihydro­pyrimidine ring exhibits an envelope conformation. The dihedral angle between the mean planes of the dihydro­pyrimidine and phenyl rings is 83.94 (6)°. The OCH(2)CH(3) group is disordered over two sites with occupancies of 0.155 (3) and 0....

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Detalles Bibliográficos
Autores principales: Mou, Jie, Yu, Chen-Xia, Yao, Chang-Sheng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983298/
https://www.ncbi.nlm.nih.gov/pubmed/21587613
http://dx.doi.org/10.1107/S1600536810037712
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author Mou, Jie
Yu, Chen-Xia
Yao, Chang-Sheng
author_facet Mou, Jie
Yu, Chen-Xia
Yao, Chang-Sheng
author_sort Mou, Jie
collection PubMed
description In the title compound, C(15)H(12)ClF(3)N(4)O(2), the dihydro­pyrimidine ring exhibits an envelope conformation. The dihedral angle between the mean planes of the dihydro­pyrimidine and phenyl rings is 83.94 (6)°. The OCH(2)CH(3) group is disordered over two sites with occupancies of 0.155 (3) and 0.845 (3). The crystal packing is stabilized by inter­molecular N—H⋯N hydrogen bonds.
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spelling pubmed-29832982010-12-30 Ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate Mou, Jie Yu, Chen-Xia Yao, Chang-Sheng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(12)ClF(3)N(4)O(2), the dihydro­pyrimidine ring exhibits an envelope conformation. The dihedral angle between the mean planes of the dihydro­pyrimidine and phenyl rings is 83.94 (6)°. The OCH(2)CH(3) group is disordered over two sites with occupancies of 0.155 (3) and 0.845 (3). The crystal packing is stabilized by inter­molecular N—H⋯N hydrogen bonds. International Union of Crystallography 2010-09-25 /pmc/articles/PMC2983298/ /pubmed/21587613 http://dx.doi.org/10.1107/S1600536810037712 Text en © Mou et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mou, Jie
Yu, Chen-Xia
Yao, Chang-Sheng
Ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate
title Ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate
title_full Ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate
title_fullStr Ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate
title_full_unstemmed Ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate
title_short Ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate
title_sort ethyl 7-(2-chloro­phen­yl)-5-trifluoro­meth­yl-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine-6-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983298/
https://www.ncbi.nlm.nih.gov/pubmed/21587613
http://dx.doi.org/10.1107/S1600536810037712
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AT yuchenxia ethyl72chlorophenyl5trifluoromethyl47dihydro124triazolo15apyrimidine6carboxylate
AT yaochangsheng ethyl72chlorophenyl5trifluoromethyl47dihydro124triazolo15apyrimidine6carboxylate

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