4-[(2-Hy­droxy­benzyl­idene)amino]-N-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph

The title compound, C(17)H(15)N(3)O(4)S, is a monoclinic polymorph with space group P2(1)/c of the previously reported triclinic form in P [Image: see text] [Subashini et al. (2009 ▶). J. Chem. Crystallogr. 39, 112–116]. In both polymorphs, intra­molecular O—H⋯N hydrogen bonds and dimer formation vi...

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Detalles Bibliográficos
Autores principales: Ebenezer, Samuel, Muthiah, Packianathan Thomas
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983326/
https://www.ncbi.nlm.nih.gov/pubmed/21587557
http://dx.doi.org/10.1107/S1600536810036585
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author Ebenezer, Samuel
Muthiah, Packianathan Thomas
author_facet Ebenezer, Samuel
Muthiah, Packianathan Thomas
author_sort Ebenezer, Samuel
collection PubMed
description The title compound, C(17)H(15)N(3)O(4)S, is a monoclinic polymorph with space group P2(1)/c of the previously reported triclinic form in P [Image: see text] [Subashini et al. (2009 ▶). J. Chem. Crystallogr. 39, 112–116]. In both polymorphs, intra­molecular O—H⋯N hydrogen bonds and dimer formation via a pair of inter­molecular N—H⋯N hydrogen bonds with an R (2) (2)(8) motif are observed. The two polymorphs differ in the next level of supra­molecular organization involving C—H⋯O hydrogen bonds with varied packing and different conformations.
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spelling pubmed-29833262010-12-30 4-[(2-Hy­droxy­benzyl­idene)amino]-N-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph Ebenezer, Samuel Muthiah, Packianathan Thomas Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(15)N(3)O(4)S, is a monoclinic polymorph with space group P2(1)/c of the previously reported triclinic form in P [Image: see text] [Subashini et al. (2009 ▶). J. Chem. Crystallogr. 39, 112–116]. In both polymorphs, intra­molecular O—H⋯N hydrogen bonds and dimer formation via a pair of inter­molecular N—H⋯N hydrogen bonds with an R (2) (2)(8) motif are observed. The two polymorphs differ in the next level of supra­molecular organization involving C—H⋯O hydrogen bonds with varied packing and different conformations. International Union of Crystallography 2010-09-18 /pmc/articles/PMC2983326/ /pubmed/21587557 http://dx.doi.org/10.1107/S1600536810036585 Text en © Ebenezer and Muthiah 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ebenezer, Samuel
Muthiah, Packianathan Thomas
4-[(2-Hy­droxy­benzyl­idene)amino]-N-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph
title 4-[(2-Hy­droxy­benzyl­idene)amino]-N-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph
title_full 4-[(2-Hy­droxy­benzyl­idene)amino]-N-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph
title_fullStr 4-[(2-Hy­droxy­benzyl­idene)amino]-N-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph
title_full_unstemmed 4-[(2-Hy­droxy­benzyl­idene)amino]-N-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph
title_short 4-[(2-Hy­droxy­benzyl­idene)amino]-N-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph
title_sort 4-[(2-hy­droxy­benzyl­idene)amino]-n-(5-methyl­isoxazol-3-yl)benzene­sulfonamide: a monoclinic polymorph
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983326/
https://www.ncbi.nlm.nih.gov/pubmed/21587557
http://dx.doi.org/10.1107/S1600536810036585
work_keys_str_mv AT ebenezersamuel 42hydroxybenzylideneaminon5methylisoxazol3ylbenzenesulfonamideamonoclinicpolymorph
AT muthiahpackianathanthomas 42hydroxybenzylideneaminon5methylisoxazol3ylbenzenesulfonamideamonoclinicpolymorph

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