Bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] N,N-dimethyl­formamide disolvate monohydrate

In the title compound, 2C(15)H(14)N(4)O(7)·2C(3)H(7)NO·H(2)O, the hydrazone mol­ecules are roughly planar, with the two benzene rings twisted slightly relative to each other by dihedral angle of 6.04 (11) and 7.75 (11)° in the two mol­ecules. The water mol­ecule is linked to the Schiff base mol­ecul...

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Detalles Bibliográficos
Autores principales: Zhao, Lin-xiu, Li, Gang-shen
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983379/
https://www.ncbi.nlm.nih.gov/pubmed/21587615
http://dx.doi.org/10.1107/S1600536810037803
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author Zhao, Lin-xiu
Li, Gang-shen
author_facet Zhao, Lin-xiu
Li, Gang-shen
author_sort Zhao, Lin-xiu
collection PubMed
description In the title compound, 2C(15)H(14)N(4)O(7)·2C(3)H(7)NO·H(2)O, the hydrazone mol­ecules are roughly planar, with the two benzene rings twisted slightly relative to each other by dihedral angle of 6.04 (11) and 7.75 (11)° in the two mol­ecules. The water mol­ecule is linked to the Schiff base mol­ecule by an O—H⋯O hydrogen bond. Intra­molecular N—H⋯O hydrogen bonds occur. In the crystal, mol­ecules are linked by inter­molecular N—H⋯O and O—H⋯O hydrogen bonds.
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spelling pubmed-29833792010-12-30 Bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] N,N-dimethyl­formamide disolvate monohydrate Zhao, Lin-xiu Li, Gang-shen Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, 2C(15)H(14)N(4)O(7)·2C(3)H(7)NO·H(2)O, the hydrazone mol­ecules are roughly planar, with the two benzene rings twisted slightly relative to each other by dihedral angle of 6.04 (11) and 7.75 (11)° in the two mol­ecules. The water mol­ecule is linked to the Schiff base mol­ecule by an O—H⋯O hydrogen bond. Intra­molecular N—H⋯O hydrogen bonds occur. In the crystal, mol­ecules are linked by inter­molecular N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2010-09-30 /pmc/articles/PMC2983379/ /pubmed/21587615 http://dx.doi.org/10.1107/S1600536810037803 Text en © Zhao and Li 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhao, Lin-xiu
Li, Gang-shen
Bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] N,N-dimethyl­formamide disolvate monohydrate
title Bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] N,N-dimethyl­formamide disolvate monohydrate
title_full Bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] N,N-dimethyl­formamide disolvate monohydrate
title_fullStr Bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] N,N-dimethyl­formamide disolvate monohydrate
title_full_unstemmed Bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] N,N-dimethyl­formamide disolvate monohydrate
title_short Bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] N,N-dimethyl­formamide disolvate monohydrate
title_sort bis[4-hy­droxy-3,5-dimeth­oxy­benzalde­hyde (2,4-dinitro­phen­yl)hydrazone] n,n-dimethyl­formamide disolvate monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983379/
https://www.ncbi.nlm.nih.gov/pubmed/21587615
http://dx.doi.org/10.1107/S1600536810037803
work_keys_str_mv AT zhaolinxiu bis4hydroxy35dimethoxybenzaldehyde24dinitrophenylhydrazonenndimethylformamidedisolvatemonohydrate
AT ligangshen bis4hydroxy35dimethoxybenzaldehyde24dinitrophenylhydrazonenndimethylformamidedisolvatemonohydrate

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