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1-Benzyl­idene-4-ethyl­thio­semicarbazide

The title compound, C(10)H(13)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and benzaldehyde. The dihedral angle between the benzene ring and the thio­urea unit is 8.96 (7)° and an intra­molecular N—H⋯N hydrogen bond generates an S(5) ring. In the crystal, inversion dimers linked...

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Detalles Bibliográficos
Autores principales: Li, Yu-Feng, Zhang, Yun-Cheng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983406/
https://www.ncbi.nlm.nih.gov/pubmed/21587654
http://dx.doi.org/10.1107/S1600536810038444
Descripción
Sumario:The title compound, C(10)H(13)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and benzaldehyde. The dihedral angle between the benzene ring and the thio­urea unit is 8.96 (7)° and an intra­molecular N—H⋯N hydrogen bond generates an S(5) ring. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops.