1-Benzyl­idene-4-ethyl­thio­semicarbazide

The title compound, C(10)H(13)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and benzaldehyde. The dihedral angle between the benzene ring and the thio­urea unit is 8.96 (7)° and an intra­molecular N—H⋯N hydrogen bond generates an S(5) ring. In the crystal, inversion dimers linked...

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Detalles Bibliográficos
Autores principales: Li, Yu-Feng, Zhang, Yun-Cheng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983406/
https://www.ncbi.nlm.nih.gov/pubmed/21587654
http://dx.doi.org/10.1107/S1600536810038444
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author Li, Yu-Feng
Zhang, Yun-Cheng
author_facet Li, Yu-Feng
Zhang, Yun-Cheng
author_sort Li, Yu-Feng
collection PubMed
description The title compound, C(10)H(13)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and benzaldehyde. The dihedral angle between the benzene ring and the thio­urea unit is 8.96 (7)° and an intra­molecular N—H⋯N hydrogen bond generates an S(5) ring. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops.
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spelling pubmed-29834062010-12-30 1-Benzyl­idene-4-ethyl­thio­semicarbazide Li, Yu-Feng Zhang, Yun-Cheng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(13)N(3)S, was prepared by the reaction of 4-ethyl­thio­semicarbazide and benzaldehyde. The dihedral angle between the benzene ring and the thio­urea unit is 8.96 (7)° and an intra­molecular N—H⋯N hydrogen bond generates an S(5) ring. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops. International Union of Crystallography 2010-09-30 /pmc/articles/PMC2983406/ /pubmed/21587654 http://dx.doi.org/10.1107/S1600536810038444 Text en © Li and Zhang 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Yu-Feng
Zhang, Yun-Cheng
1-Benzyl­idene-4-ethyl­thio­semicarbazide
title 1-Benzyl­idene-4-ethyl­thio­semicarbazide
title_full 1-Benzyl­idene-4-ethyl­thio­semicarbazide
title_fullStr 1-Benzyl­idene-4-ethyl­thio­semicarbazide
title_full_unstemmed 1-Benzyl­idene-4-ethyl­thio­semicarbazide
title_short 1-Benzyl­idene-4-ethyl­thio­semicarbazide
title_sort 1-benzyl­idene-4-ethyl­thio­semicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983406/
https://www.ncbi.nlm.nih.gov/pubmed/21587654
http://dx.doi.org/10.1107/S1600536810038444
work_keys_str_mv AT liyufeng 1benzylidene4ethylthiosemicarbazide
AT zhangyuncheng 1benzylidene4ethylthiosemicarbazide

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