Carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data

In the cation of the title compound, C(24)H(27)N(2)O(4) (+)·H(2)PO(4) (−)·C(3)H(8)O [systematic name: 3-(9H-carbazol-4-yl­oxy)-2-hydr­oxy-N-[2-(2-methoxy­phen­oxy)eth­yl]propan-1-aminium dihydro­gen phosphate propan-2-ol solvate], the mean planes of the tricyclic carbazole system and the benzene rin...

Descripción completa

Detalles Bibliográficos
Autores principales: Chernyshev, Vladimir V., Kukushkin, Sergei Yu., Velikodny, Yurii A.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983528/
https://www.ncbi.nlm.nih.gov/pubmed/21580371
http://dx.doi.org/10.1107/S1600536810005349
_version_ 1782191893808939008
author Chernyshev, Vladimir V.
Kukushkin, Sergei Yu.
Velikodny, Yurii A.
author_facet Chernyshev, Vladimir V.
Kukushkin, Sergei Yu.
Velikodny, Yurii A.
author_sort Chernyshev, Vladimir V.
collection PubMed
description In the cation of the title compound, C(24)H(27)N(2)O(4) (+)·H(2)PO(4) (−)·C(3)H(8)O [systematic name: 3-(9H-carbazol-4-yl­oxy)-2-hydr­oxy-N-[2-(2-methoxy­phen­oxy)eth­yl]propan-1-aminium dihydro­gen phosphate propan-2-ol solvate], the mean planes of the tricyclic carbazole system and the benzene ring form a dihedral angle of 42.00 (16)°. In the crystal structure, classical inter­molecular O—H⋯O and N—H⋯O hydrogen bonds link the cations, anions and solvent mol­ecules into layers parallel to the ac plane.
format Text
id pubmed-2983528
institution National Center for Biotechnology Information
language English
publishDate 2010
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29835282010-12-30 Carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data Chernyshev, Vladimir V. Kukushkin, Sergei Yu. Velikodny, Yurii A. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the cation of the title compound, C(24)H(27)N(2)O(4) (+)·H(2)PO(4) (−)·C(3)H(8)O [systematic name: 3-(9H-carbazol-4-yl­oxy)-2-hydr­oxy-N-[2-(2-methoxy­phen­oxy)eth­yl]propan-1-aminium dihydro­gen phosphate propan-2-ol solvate], the mean planes of the tricyclic carbazole system and the benzene ring form a dihedral angle of 42.00 (16)°. In the crystal structure, classical inter­molecular O—H⋯O and N—H⋯O hydrogen bonds link the cations, anions and solvent mol­ecules into layers parallel to the ac plane. International Union of Crystallography 2010-02-13 /pmc/articles/PMC2983528/ /pubmed/21580371 http://dx.doi.org/10.1107/S1600536810005349 Text en © Chernyshev et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chernyshev, Vladimir V.
Kukushkin, Sergei Yu.
Velikodny, Yurii A.
Carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data
title Carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data
title_full Carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data
title_fullStr Carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data
title_full_unstemmed Carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data
title_short Carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data
title_sort carvedilol dihydrogen phosphate propan-2-ol solvate from powder diffraction data
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983528/
https://www.ncbi.nlm.nih.gov/pubmed/21580371
http://dx.doi.org/10.1107/S1600536810005349
work_keys_str_mv AT chernyshevvladimirv carvediloldihydrogenphosphatepropan2olsolvatefrompowderdiffractiondata
AT kukushkinsergeiyu carvediloldihydrogenphosphatepropan2olsolvatefrompowderdiffractiondata
AT velikodnyyuriia carvediloldihydrogenphosphatepropan2olsolvatefrompowderdiffractiondata

Ejemplares similares