N-(3-Chloro­propion­yl)-N′-phenyl­thio­urea

The title compound, C(10)H(11)ClN(2)OS, adopts a cis-trans configuration with respect to the position of the phenyl and 3-chloro­propionyl groups relative to the thiono group across the C—N bonds. The benzene ring is perpendicular to the propionyl thio­urea fragment with a dihedral angle of 82.62 (1...

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Detalles Bibliográficos
Autores principales: Othman, Eliyanti A., Soh, Siti K. C., Yamin, Bohari M.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983529/
https://www.ncbi.nlm.nih.gov/pubmed/21580385
http://dx.doi.org/10.1107/S1600536810005271
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author Othman, Eliyanti A.
Soh, Siti K. C.
Yamin, Bohari M.
author_facet Othman, Eliyanti A.
Soh, Siti K. C.
Yamin, Bohari M.
author_sort Othman, Eliyanti A.
collection PubMed
description The title compound, C(10)H(11)ClN(2)OS, adopts a cis-trans configuration with respect to the position of the phenyl and 3-chloro­propionyl groups relative to the thiono group across the C—N bonds. The benzene ring is perpendicular to the propionyl thio­urea fragment with a dihedral angle of 82.62 (10)°. An intra­molecular N—H⋯O inter­action occurs. The crystal structure is stabilized by inter­molecular N—H⋯S hydrogen bonds, which link pairs of mol­ecules, building up R (2) (2)(8) ring motifs, and C—H.. π inter­actions.
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spelling pubmed-29835292010-12-30 N-(3-Chloro­propion­yl)-N′-phenyl­thio­urea Othman, Eliyanti A. Soh, Siti K. C. Yamin, Bohari M. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(11)ClN(2)OS, adopts a cis-trans configuration with respect to the position of the phenyl and 3-chloro­propionyl groups relative to the thiono group across the C—N bonds. The benzene ring is perpendicular to the propionyl thio­urea fragment with a dihedral angle of 82.62 (10)°. An intra­molecular N—H⋯O inter­action occurs. The crystal structure is stabilized by inter­molecular N—H⋯S hydrogen bonds, which link pairs of mol­ecules, building up R (2) (2)(8) ring motifs, and C—H.. π inter­actions. International Union of Crystallography 2010-02-13 /pmc/articles/PMC2983529/ /pubmed/21580385 http://dx.doi.org/10.1107/S1600536810005271 Text en © Othman et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Othman, Eliyanti A.
Soh, Siti K. C.
Yamin, Bohari M.
N-(3-Chloro­propion­yl)-N′-phenyl­thio­urea
title N-(3-Chloro­propion­yl)-N′-phenyl­thio­urea
title_full N-(3-Chloro­propion­yl)-N′-phenyl­thio­urea
title_fullStr N-(3-Chloro­propion­yl)-N′-phenyl­thio­urea
title_full_unstemmed N-(3-Chloro­propion­yl)-N′-phenyl­thio­urea
title_short N-(3-Chloro­propion­yl)-N′-phenyl­thio­urea
title_sort n-(3-chloro­propion­yl)-n′-phenyl­thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983529/
https://www.ncbi.nlm.nih.gov/pubmed/21580385
http://dx.doi.org/10.1107/S1600536810005271
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AT sohsitikc n3chloropropionylnphenylthiourea
AT yaminboharim n3chloropropionylnphenylthiourea

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