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N′-(2-Methoxy-1-naphthylidene)nicotinohydrazide
The title compound, C(18)H(15)N(3)O(2), was prepared by the reaction of 2-methoxynaphthaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the naphthalene ring system and the pyridine ring is 9.2 (3)°. An intramolecular C—H⋯N hydrogen bond is observed. In the crystal str...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2010
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983545/ https://www.ncbi.nlm.nih.gov/pubmed/21580294 http://dx.doi.org/10.1107/S1600536810003843 |
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author | Li, Cong Wang, Ping Su, Yong-Qing |
author_facet | Li, Cong Wang, Ping Su, Yong-Qing |
author_sort | Li, Cong |
collection | PubMed |
description | The title compound, C(18)H(15)N(3)O(2), was prepared by the reaction of 2-methoxynaphthaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the naphthalene ring system and the pyridine ring is 9.2 (3)°. An intramolecular C—H⋯N hydrogen bond is observed. In the crystal structure, molecules are linked into chains running along the c axis by intermolecular N—H⋯O hydrogen bonds. |
format | Text |
id | pubmed-2983545 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2010 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29835452010-12-30 N′-(2-Methoxy-1-naphthylidene)nicotinohydrazide Li, Cong Wang, Ping Su, Yong-Qing Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(15)N(3)O(2), was prepared by the reaction of 2-methoxynaphthaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the naphthalene ring system and the pyridine ring is 9.2 (3)°. An intramolecular C—H⋯N hydrogen bond is observed. In the crystal structure, molecules are linked into chains running along the c axis by intermolecular N—H⋯O hydrogen bonds. International Union of Crystallography 2010-02-06 /pmc/articles/PMC2983545/ /pubmed/21580294 http://dx.doi.org/10.1107/S1600536810003843 Text en © Li et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Li, Cong Wang, Ping Su, Yong-Qing N′-(2-Methoxy-1-naphthylidene)nicotinohydrazide |
title |
N′-(2-Methoxy-1-naphthylidene)nicotinohydrazide |
title_full |
N′-(2-Methoxy-1-naphthylidene)nicotinohydrazide |
title_fullStr |
N′-(2-Methoxy-1-naphthylidene)nicotinohydrazide |
title_full_unstemmed |
N′-(2-Methoxy-1-naphthylidene)nicotinohydrazide |
title_short |
N′-(2-Methoxy-1-naphthylidene)nicotinohydrazide |
title_sort | n′-(2-methoxy-1-naphthylidene)nicotinohydrazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983545/ https://www.ncbi.nlm.nih.gov/pubmed/21580294 http://dx.doi.org/10.1107/S1600536810003843 |
work_keys_str_mv | AT licong n2methoxy1naphthylidenenicotinohydrazide AT wangping n2methoxy1naphthylidenenicotinohydrazide AT suyongqing n2methoxy1naphthylidenenicotinohydrazide |