2,4-Bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one

The title compound, C(21)H(21)Cl(2)NO, exists in a twin-chair conformation with an equatorial orientation of the 4-chloro­phenyl groups on both sides of the secondary amino group; the dihedral angle between the 4-chloro­phenyl rings is 36.58 (2)°. The crystal packing is stabilized by an inter­molecu...

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Detalles Bibliográficos
Autores principales: Parthiban, P., Ramkumar, V., Jeong, Yeon Tae
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983554/
https://www.ncbi.nlm.nih.gov/pubmed/21580316
http://dx.doi.org/10.1107/S1600536810004095
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author Parthiban, P.
Ramkumar, V.
Jeong, Yeon Tae
author_facet Parthiban, P.
Ramkumar, V.
Jeong, Yeon Tae
author_sort Parthiban, P.
collection PubMed
description The title compound, C(21)H(21)Cl(2)NO, exists in a twin-chair conformation with an equatorial orientation of the 4-chloro­phenyl groups on both sides of the secondary amino group; the dihedral angle between the 4-chloro­phenyl rings is 36.58 (2)°. The crystal packing is stabilized by an inter­molecular N—H⋯O hydrogen bond and a weak Cl⋯Cl [3.4331 (9) Å] inter­action.
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spelling pubmed-29835542010-12-30 2,4-Bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one Parthiban, P. Ramkumar, V. Jeong, Yeon Tae Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(21)H(21)Cl(2)NO, exists in a twin-chair conformation with an equatorial orientation of the 4-chloro­phenyl groups on both sides of the secondary amino group; the dihedral angle between the 4-chloro­phenyl rings is 36.58 (2)°. The crystal packing is stabilized by an inter­molecular N—H⋯O hydrogen bond and a weak Cl⋯Cl [3.4331 (9) Å] inter­action. International Union of Crystallography 2010-02-06 /pmc/articles/PMC2983554/ /pubmed/21580316 http://dx.doi.org/10.1107/S1600536810004095 Text en © Parthiban et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Parthiban, P.
Ramkumar, V.
Jeong, Yeon Tae
2,4-Bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one
title 2,4-Bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one
title_full 2,4-Bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one
title_fullStr 2,4-Bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one
title_full_unstemmed 2,4-Bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one
title_short 2,4-Bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one
title_sort 2,4-bis(4-chloro­phen­yl)-1-methyl-3-aza­bicyclo­[3.3.1]nonan-9-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983554/
https://www.ncbi.nlm.nih.gov/pubmed/21580316
http://dx.doi.org/10.1107/S1600536810004095
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