N′-[1-(5-Bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate

The benzohydrazide mol­ecule in the title compound, C(15)H(13)BrN(2)O(5)·C(2)H(6)OS·3H(2)O, is almost planar with an r.m.s. deviation for the non-H atoms of 0.078 Å. The organic mol­ecules, water and dimethyl sulfoxide solvent mol­ecules are linked by N—H⋯O, O—H⋯O and O—H⋯S inter­molecular hydrogen...

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Detalles Bibliográficos
Autores principales: Suleiman Gwaram, Nura, Khaledi, Hamid, Mohd Ali, Hapipah, Robinson, Ward T., Abdulla, Mahmood A.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983555/
https://www.ncbi.nlm.nih.gov/pubmed/21580457
http://dx.doi.org/10.1107/S1600536810007002
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author Suleiman Gwaram, Nura
Khaledi, Hamid
Mohd Ali, Hapipah
Robinson, Ward T.
Abdulla, Mahmood A.
author_facet Suleiman Gwaram, Nura
Khaledi, Hamid
Mohd Ali, Hapipah
Robinson, Ward T.
Abdulla, Mahmood A.
author_sort Suleiman Gwaram, Nura
collection PubMed
description The benzohydrazide mol­ecule in the title compound, C(15)H(13)BrN(2)O(5)·C(2)H(6)OS·3H(2)O, is almost planar with an r.m.s. deviation for the non-H atoms of 0.078 Å. The organic mol­ecules, water and dimethyl sulfoxide solvent mol­ecules are linked by N—H⋯O, O—H⋯O and O—H⋯S inter­molecular hydrogen bonds, forming zigzag chains along the a axis. Intra­molecular O—H⋯O and O—H⋯N hydrogen bonds also occur.
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spelling pubmed-29835552010-12-30 N′-[1-(5-Bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate Suleiman Gwaram, Nura Khaledi, Hamid Mohd Ali, Hapipah Robinson, Ward T. Abdulla, Mahmood A. Acta Crystallogr Sect E Struct Rep Online Organic Papers The benzohydrazide mol­ecule in the title compound, C(15)H(13)BrN(2)O(5)·C(2)H(6)OS·3H(2)O, is almost planar with an r.m.s. deviation for the non-H atoms of 0.078 Å. The organic mol­ecules, water and dimethyl sulfoxide solvent mol­ecules are linked by N—H⋯O, O—H⋯O and O—H⋯S inter­molecular hydrogen bonds, forming zigzag chains along the a axis. Intra­molecular O—H⋯O and O—H⋯N hydrogen bonds also occur. International Union of Crystallography 2010-02-27 /pmc/articles/PMC2983555/ /pubmed/21580457 http://dx.doi.org/10.1107/S1600536810007002 Text en © Suleiman Gwaram et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Suleiman Gwaram, Nura
Khaledi, Hamid
Mohd Ali, Hapipah
Robinson, Ward T.
Abdulla, Mahmood A.
N′-[1-(5-Bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate
title N′-[1-(5-Bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate
title_full N′-[1-(5-Bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate
title_fullStr N′-[1-(5-Bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate
title_full_unstemmed N′-[1-(5-Bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate
title_short N′-[1-(5-Bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate
title_sort n′-[1-(5-bromo-2-hydroxy­phen­yl)ethyl­idene]-3,4,5-trihydroxy­benzohydrazide dimethyl sulfoxide solvate trihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983555/
https://www.ncbi.nlm.nih.gov/pubmed/21580457
http://dx.doi.org/10.1107/S1600536810007002
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