Ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1H,5H-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate

In the title mol­ecule, C(37)H(35)N(3)O(6), the pyrrolidine ring adopts a twist conformation and the piperidine ring is in a distorted boat conformation. One of the phenyl rings is disordered over two positions with occupancies of 0.54 (2) and 0.46 (2) and the ethyl carboxyl­ate group is also disord...

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Autores principales: Sundaresan, S. S., Ramesh, P., Arumugam, N., Raghunathan, R., Ponnuswamy, M. N.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983610/
https://www.ncbi.nlm.nih.gov/pubmed/21580400
http://dx.doi.org/10.1107/S1600536810005696
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author Sundaresan, S. S.
Ramesh, P.
Arumugam, N.
Raghunathan, R.
Ponnuswamy, M. N.
author_facet Sundaresan, S. S.
Ramesh, P.
Arumugam, N.
Raghunathan, R.
Ponnuswamy, M. N.
author_sort Sundaresan, S. S.
collection PubMed
description In the title mol­ecule, C(37)H(35)N(3)O(6), the pyrrolidine ring adopts a twist conformation and the piperidine ring is in a distorted boat conformation. One of the phenyl rings is disordered over two positions with occupancies of 0.54 (2) and 0.46 (2) and the ethyl carboxyl­ate group is also disordered over two orientations with occupancies of 0.75 (1) and 0.25 (1).
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spelling pubmed-29836102010-12-30 Ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1H,5H-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate Sundaresan, S. S. Ramesh, P. Arumugam, N. Raghunathan, R. Ponnuswamy, M. N. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title mol­ecule, C(37)H(35)N(3)O(6), the pyrrolidine ring adopts a twist conformation and the piperidine ring is in a distorted boat conformation. One of the phenyl rings is disordered over two positions with occupancies of 0.54 (2) and 0.46 (2) and the ethyl carboxyl­ate group is also disordered over two orientations with occupancies of 0.75 (1) and 0.25 (1). International Union of Crystallography 2010-02-17 /pmc/articles/PMC2983610/ /pubmed/21580400 http://dx.doi.org/10.1107/S1600536810005696 Text en © Sundaresan et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Sundaresan, S. S.
Ramesh, P.
Arumugam, N.
Raghunathan, R.
Ponnuswamy, M. N.
Ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1H,5H-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate
title Ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1H,5H-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate
title_full Ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1H,5H-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate
title_fullStr Ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1H,5H-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate
title_full_unstemmed Ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1H,5H-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate
title_short Ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1H,5H-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate
title_sort ethyl 3-[1-(4-methoxy­phen­yl)-4-oxo-3-phenylazetidin-2-yl]-2-nitro-1-phenyl-2,3,10,10a-tetra­hydro-1h,5h-pyrrolo[1,2-b]isoquinoline-10a-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983610/
https://www.ncbi.nlm.nih.gov/pubmed/21580400
http://dx.doi.org/10.1107/S1600536810005696
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