Diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate

In the title compound, C(21)H(28)N(2)O(4), the dihydro­pyridine ring adopts a flattened boat conformation. The mean plane of the dihydro­pyridine ring and the attached benzene ring form a dihedral angle of 85.1 (1) Å. One of two ethyl fragments is disordered between two conformations in a 0.67 (4):0...

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Detalles Bibliográficos
Autores principales: Ji, Xiao-Ling, Sun, Wang-Bin, Zhang, Qian, Cao, Yan-Ping, Bai, Ming-Sheng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983663/
https://www.ncbi.nlm.nih.gov/pubmed/21580293
http://dx.doi.org/10.1107/S1600536810003508
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author Ji, Xiao-Ling
Sun, Wang-Bin
Zhang, Qian
Cao, Yan-Ping
Bai, Ming-Sheng
author_facet Ji, Xiao-Ling
Sun, Wang-Bin
Zhang, Qian
Cao, Yan-Ping
Bai, Ming-Sheng
author_sort Ji, Xiao-Ling
collection PubMed
description In the title compound, C(21)H(28)N(2)O(4), the dihydro­pyridine ring adopts a flattened boat conformation. The mean plane of the dihydro­pyridine ring and the attached benzene ring form a dihedral angle of 85.1 (1) Å. One of two ethyl fragments is disordered between two conformations in a 0.67 (4):0.33 (4) ratio. In the crystal structure, mol­ecules related by translation along the a axis are linked into chains via inter­molecular N—H⋯O hydrogen bonds.
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spelling pubmed-29836632010-12-30 Diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate Ji, Xiao-Ling Sun, Wang-Bin Zhang, Qian Cao, Yan-Ping Bai, Ming-Sheng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(21)H(28)N(2)O(4), the dihydro­pyridine ring adopts a flattened boat conformation. The mean plane of the dihydro­pyridine ring and the attached benzene ring form a dihedral angle of 85.1 (1) Å. One of two ethyl fragments is disordered between two conformations in a 0.67 (4):0.33 (4) ratio. In the crystal structure, mol­ecules related by translation along the a axis are linked into chains via inter­molecular N—H⋯O hydrogen bonds. International Union of Crystallography 2010-02-06 /pmc/articles/PMC2983663/ /pubmed/21580293 http://dx.doi.org/10.1107/S1600536810003508 Text en © Ji et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ji, Xiao-Ling
Sun, Wang-Bin
Zhang, Qian
Cao, Yan-Ping
Bai, Ming-Sheng
Diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate
title Diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate
title_full Diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate
title_fullStr Diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate
title_full_unstemmed Diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate
title_short Diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate
title_sort diethyl 4-[4-(dimethyl­amino)phen­yl]-2,6-dimethyl-1,4-dihydro­pyridine-3,5-dicarboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983663/
https://www.ncbi.nlm.nih.gov/pubmed/21580293
http://dx.doi.org/10.1107/S1600536810003508
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