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2-(2,7-Dimeth­oxy-1-naphtho­yl)benzoic acid

In the title compound, C(20)H(16)O(5), the dihedral angle between the naphthalene ring system and the benzene ring is 67.43 (5)°. The bridging carbonyl C—C(=O)—C plane makes dihedral angles of 82.64 (6) and 41.79 (7)°, respectively, with the naphthalene ring system and the benzene ring. The dihedral...

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Autores principales: Hijikata, Daichi, Nakaema, Kosuke, Watanabe, Shoji, Okamoto, Akiko, Yonezawa, Noriyuki
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983668/
https://www.ncbi.nlm.nih.gov/pubmed/21580451
http://dx.doi.org/10.1107/S1600536810006847
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author Hijikata, Daichi
Nakaema, Kosuke
Watanabe, Shoji
Okamoto, Akiko
Yonezawa, Noriyuki
author_facet Hijikata, Daichi
Nakaema, Kosuke
Watanabe, Shoji
Okamoto, Akiko
Yonezawa, Noriyuki
author_sort Hijikata, Daichi
collection PubMed
description In the title compound, C(20)H(16)O(5), the dihedral angle between the naphthalene ring system and the benzene ring is 67.43 (5)°. The bridging carbonyl C—C(=O)—C plane makes dihedral angles of 82.64 (6) and 41.79 (7)°, respectively, with the naphthalene ring system and the benzene ring. The dihedral angle between the carb­oxy O—C(=O)—C plane and the benzene ring is 36.38 (7)° and that between the bridging carbonyl C—C(=O)—C plane and the carb­oxy O—C(=O)—C plane is 51.88 (8)°. The crystal structure is stabilized by inter­molecular O—H⋯O and C—H⋯O hydrogen-bonding inter­actions. An intra­molecular C—H⋯O hydrogen bond occurs between a naphthalene H atom and the carbonyl O atom of the carb­oxy group.
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spelling pubmed-29836682010-12-30 2-(2,7-Dimeth­oxy-1-naphtho­yl)benzoic acid Hijikata, Daichi Nakaema, Kosuke Watanabe, Shoji Okamoto, Akiko Yonezawa, Noriyuki Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(20)H(16)O(5), the dihedral angle between the naphthalene ring system and the benzene ring is 67.43 (5)°. The bridging carbonyl C—C(=O)—C plane makes dihedral angles of 82.64 (6) and 41.79 (7)°, respectively, with the naphthalene ring system and the benzene ring. The dihedral angle between the carb­oxy O—C(=O)—C plane and the benzene ring is 36.38 (7)° and that between the bridging carbonyl C—C(=O)—C plane and the carb­oxy O—C(=O)—C plane is 51.88 (8)°. The crystal structure is stabilized by inter­molecular O—H⋯O and C—H⋯O hydrogen-bonding inter­actions. An intra­molecular C—H⋯O hydrogen bond occurs between a naphthalene H atom and the carbonyl O atom of the carb­oxy group. International Union of Crystallography 2010-02-27 /pmc/articles/PMC2983668/ /pubmed/21580451 http://dx.doi.org/10.1107/S1600536810006847 Text en © Hijikata et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hijikata, Daichi
Nakaema, Kosuke
Watanabe, Shoji
Okamoto, Akiko
Yonezawa, Noriyuki
2-(2,7-Dimeth­oxy-1-naphtho­yl)benzoic acid
title 2-(2,7-Dimeth­oxy-1-naphtho­yl)benzoic acid
title_full 2-(2,7-Dimeth­oxy-1-naphtho­yl)benzoic acid
title_fullStr 2-(2,7-Dimeth­oxy-1-naphtho­yl)benzoic acid
title_full_unstemmed 2-(2,7-Dimeth­oxy-1-naphtho­yl)benzoic acid
title_short 2-(2,7-Dimeth­oxy-1-naphtho­yl)benzoic acid
title_sort 2-(2,7-dimeth­oxy-1-naphtho­yl)benzoic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983668/
https://www.ncbi.nlm.nih.gov/pubmed/21580451
http://dx.doi.org/10.1107/S1600536810006847
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