N′-(2-Methoxy­benzyl­idene)nicotinohydrazide

The title compound, C(14)H(13)N(3)O(2), was prepared by the reaction of 2-methoxy­benzyaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the benzene and pyridine rings is 5.9 (3)°. In the crystal structure, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds, l...

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Detalles Bibliográficos
Autores principales: Wang, Ping, Li, Cong, Su, Yong-Qing
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983706/
https://www.ncbi.nlm.nih.gov/pubmed/21580313
http://dx.doi.org/10.1107/S1600536810003831
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author Wang, Ping
Li, Cong
Su, Yong-Qing
author_facet Wang, Ping
Li, Cong
Su, Yong-Qing
author_sort Wang, Ping
collection PubMed
description The title compound, C(14)H(13)N(3)O(2), was prepared by the reaction of 2-methoxy­benzyaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the benzene and pyridine rings is 5.9 (3)°. In the crystal structure, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds, leading to the formation of chains along the c axis; adjacent chains are linked via C—H⋯O and C—H⋯N hydrogen bonds.
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spelling pubmed-29837062010-12-30 N′-(2-Methoxy­benzyl­idene)nicotinohydrazide Wang, Ping Li, Cong Su, Yong-Qing Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(13)N(3)O(2), was prepared by the reaction of 2-methoxy­benzyaldehyde with nicotinic acid hydrazide in methanol. The dihedral angle between the benzene and pyridine rings is 5.9 (3)°. In the crystal structure, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds, leading to the formation of chains along the c axis; adjacent chains are linked via C—H⋯O and C—H⋯N hydrogen bonds. International Union of Crystallography 2010-02-06 /pmc/articles/PMC2983706/ /pubmed/21580313 http://dx.doi.org/10.1107/S1600536810003831 Text en © Wang et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Ping
Li, Cong
Su, Yong-Qing
N′-(2-Methoxy­benzyl­idene)nicotinohydrazide
title N′-(2-Methoxy­benzyl­idene)nicotinohydrazide
title_full N′-(2-Methoxy­benzyl­idene)nicotinohydrazide
title_fullStr N′-(2-Methoxy­benzyl­idene)nicotinohydrazide
title_full_unstemmed N′-(2-Methoxy­benzyl­idene)nicotinohydrazide
title_short N′-(2-Methoxy­benzyl­idene)nicotinohydrazide
title_sort n′-(2-methoxy­benzyl­idene)nicotinohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983706/
https://www.ncbi.nlm.nih.gov/pubmed/21580313
http://dx.doi.org/10.1107/S1600536810003831
work_keys_str_mv AT wangping n2methoxybenzylidenenicotinohydrazide
AT licong n2methoxybenzylidenenicotinohydrazide
AT suyongqing n2methoxybenzylidenenicotinohydrazide

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