4,4,6-Trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1H)-thione

The asymmetric unit of the title compound, C(14)H(18)N(2)S, contains two independent and conformationally similar mol­ecules, which form cyclic dimers via inter­molecular hydrogen bonds of the type N—H⋯S [graph set R (2) (2)(8)]. The structure is iso­morphous with that of one of the polymorphs of 4,...

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Detalles Bibliográficos
Autores principales: Saeed, Aamer, Khera, Rasheed Ahmad, Parvez, Masood
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983710/
https://www.ncbi.nlm.nih.gov/pubmed/21580391
http://dx.doi.org/10.1107/S1600536810004708
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author Saeed, Aamer
Khera, Rasheed Ahmad
Parvez, Masood
author_facet Saeed, Aamer
Khera, Rasheed Ahmad
Parvez, Masood
author_sort Saeed, Aamer
collection PubMed
description The asymmetric unit of the title compound, C(14)H(18)N(2)S, contains two independent and conformationally similar mol­ecules, which form cyclic dimers via inter­molecular hydrogen bonds of the type N—H⋯S [graph set R (2) (2)(8)]. The structure is iso­morphous with that of one of the polymorphs of 4,4,6-tri­methyl-1-phenyl-3,4-dihydro­pyrimidine-2(1H)-thione [Yam­in et al. (2005 ▶). Acta Cryst. E61, o55–o57].
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spelling pubmed-29837102010-12-30 4,4,6-Trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1H)-thione Saeed, Aamer Khera, Rasheed Ahmad Parvez, Masood Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(14)H(18)N(2)S, contains two independent and conformationally similar mol­ecules, which form cyclic dimers via inter­molecular hydrogen bonds of the type N—H⋯S [graph set R (2) (2)(8)]. The structure is iso­morphous with that of one of the polymorphs of 4,4,6-tri­methyl-1-phenyl-3,4-dihydro­pyrimidine-2(1H)-thione [Yam­in et al. (2005 ▶). Acta Cryst. E61, o55–o57]. International Union of Crystallography 2010-02-13 /pmc/articles/PMC2983710/ /pubmed/21580391 http://dx.doi.org/10.1107/S1600536810004708 Text en © Saeed et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saeed, Aamer
Khera, Rasheed Ahmad
Parvez, Masood
4,4,6-Trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1H)-thione
title 4,4,6-Trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1H)-thione
title_full 4,4,6-Trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1H)-thione
title_fullStr 4,4,6-Trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1H)-thione
title_full_unstemmed 4,4,6-Trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1H)-thione
title_short 4,4,6-Trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1H)-thione
title_sort 4,4,6-trimethyl-1-(3-methyl­phen­yl)-3,4-dihydro­pyrimidine-2(1h)-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983710/
https://www.ncbi.nlm.nih.gov/pubmed/21580391
http://dx.doi.org/10.1107/S1600536810004708
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