4-{3-[Hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzene­sulfonamide

In the title compound, C(15)H(14)N(4)O(3)S(2), the hydr­oxy group is disordered over two positions with occupancies of 0.619 (5) and 0.381 (5). The benzene ring attached to the heterocycle makes a dihedral angle of 86.92 (9)° with respect to the best plane through the five-membered ring. The crystal...

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Detalles Bibliográficos
Autores principales: Akkurt, Mehmet, Çelik, Ísmail, Cihan, Gökçe, Çapan, Gültaze, Büyükgüngör, Orhan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983783/
https://www.ncbi.nlm.nih.gov/pubmed/21580773
http://dx.doi.org/10.1107/S1600536810011402
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author Akkurt, Mehmet
Çelik, Ísmail
Cihan, Gökçe
Çapan, Gültaze
Büyükgüngör, Orhan
author_facet Akkurt, Mehmet
Çelik, Ísmail
Cihan, Gökçe
Çapan, Gültaze
Büyükgüngör, Orhan
author_sort Akkurt, Mehmet
collection PubMed
description In the title compound, C(15)H(14)N(4)O(3)S(2), the hydr­oxy group is disordered over two positions with occupancies of 0.619 (5) and 0.381 (5). The benzene ring attached to the heterocycle makes a dihedral angle of 86.92 (9)° with respect to the best plane through the five-membered ring. The crystal packing is stabilized by inter­molecular O—H⋯O, N—H⋯S, N—H⋯N, C—H⋯O and C—H⋯N hydrogen bonds, and N—H⋯π and C—H⋯π inter­actions.
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spelling pubmed-29837832010-12-30 4-{3-[Hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzene­sulfonamide Akkurt, Mehmet Çelik, Ísmail Cihan, Gökçe Çapan, Gültaze Büyükgüngör, Orhan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(14)N(4)O(3)S(2), the hydr­oxy group is disordered over two positions with occupancies of 0.619 (5) and 0.381 (5). The benzene ring attached to the heterocycle makes a dihedral angle of 86.92 (9)° with respect to the best plane through the five-membered ring. The crystal packing is stabilized by inter­molecular O—H⋯O, N—H⋯S, N—H⋯N, C—H⋯O and C—H⋯N hydrogen bonds, and N—H⋯π and C—H⋯π inter­actions. International Union of Crystallography 2010-03-27 /pmc/articles/PMC2983783/ /pubmed/21580773 http://dx.doi.org/10.1107/S1600536810011402 Text en © Akkurt et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Akkurt, Mehmet
Çelik, Ísmail
Cihan, Gökçe
Çapan, Gültaze
Büyükgüngör, Orhan
4-{3-[Hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzene­sulfonamide
title 4-{3-[Hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzene­sulfonamide
title_full 4-{3-[Hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzene­sulfonamide
title_fullStr 4-{3-[Hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzene­sulfonamide
title_full_unstemmed 4-{3-[Hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzene­sulfonamide
title_short 4-{3-[Hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzene­sulfonamide
title_sort 4-{3-[hydr­oxy(phen­yl)meth­yl]-5-thioxo-4,5-dihydro-1h-1,2,4-triazol-4-yl}benzene­sulfonamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983783/
https://www.ncbi.nlm.nih.gov/pubmed/21580773
http://dx.doi.org/10.1107/S1600536810011402
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