Alaptide from synchrotron powder diffraction data

The title compound [systematic name: (8S)-8-methyl-6,9-diaza­spiro­[4.5]decane-7,10-dione], C(9)H(14)N(2)O(2), consists of two connected rings, viz. a piperazine-2,5-dione (DKP) ring and a five-membered ring. The DKP ring adopts a slight boat conformation and the bonded methyl group is in an equator...

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Detalles Bibliográficos
Autores principales: Rohlíček, Jan, Maixner, Jaroslav, Pažout, Richard, Hušák, Michal, Cibulková, Jana, Kratochvíl, Bohumil
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983785/
https://www.ncbi.nlm.nih.gov/pubmed/21580652
http://dx.doi.org/10.1107/S1600536810007750
Descripción
Sumario:The title compound [systematic name: (8S)-8-methyl-6,9-diaza­spiro­[4.5]decane-7,10-dione], C(9)H(14)N(2)O(2), consists of two connected rings, viz. a piperazine-2,5-dione (DKP) ring and a five-membered ring. The DKP ring adopts a slight boat conformation and the bonded methyl group is in an equatorial position. The five-membered ring is in an envelope conformation. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into chains running parallel to the c axis.

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