Alaptide from synchrotron powder diffraction data

The title compound [systematic name: (8S)-8-methyl-6,9-diaza­spiro­[4.5]decane-7,10-dione], C(9)H(14)N(2)O(2), consists of two connected rings, viz. a piperazine-2,5-dione (DKP) ring and a five-membered ring. The DKP ring adopts a slight boat conformation and the bonded methyl group is in an equator...

Descripción completa

Detalles Bibliográficos
Autores principales: Rohlíček, Jan, Maixner, Jaroslav, Pažout, Richard, Hušák, Michal, Cibulková, Jana, Kratochvíl, Bohumil
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983785/
https://www.ncbi.nlm.nih.gov/pubmed/21580652
http://dx.doi.org/10.1107/S1600536810007750
_version_ 1782191957223669760
author Rohlíček, Jan
Maixner, Jaroslav
Pažout, Richard
Hušák, Michal
Cibulková, Jana
Kratochvíl, Bohumil
author_facet Rohlíček, Jan
Maixner, Jaroslav
Pažout, Richard
Hušák, Michal
Cibulková, Jana
Kratochvíl, Bohumil
author_sort Rohlíček, Jan
collection PubMed
description The title compound [systematic name: (8S)-8-methyl-6,9-diaza­spiro­[4.5]decane-7,10-dione], C(9)H(14)N(2)O(2), consists of two connected rings, viz. a piperazine-2,5-dione (DKP) ring and a five-membered ring. The DKP ring adopts a slight boat conformation and the bonded methyl group is in an equatorial position. The five-membered ring is in an envelope conformation. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into chains running parallel to the c axis.
format Text
id pubmed-2983785
institution National Center for Biotechnology Information
language English
publishDate 2010
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29837852010-12-30 Alaptide from synchrotron powder diffraction data Rohlíček, Jan Maixner, Jaroslav Pažout, Richard Hušák, Michal Cibulková, Jana Kratochvíl, Bohumil Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound [systematic name: (8S)-8-methyl-6,9-diaza­spiro­[4.5]decane-7,10-dione], C(9)H(14)N(2)O(2), consists of two connected rings, viz. a piperazine-2,5-dione (DKP) ring and a five-membered ring. The DKP ring adopts a slight boat conformation and the bonded methyl group is in an equatorial position. The five-membered ring is in an envelope conformation. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into chains running parallel to the c axis. International Union of Crystallography 2010-03-13 /pmc/articles/PMC2983785/ /pubmed/21580652 http://dx.doi.org/10.1107/S1600536810007750 Text en © Rohlíček et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Rohlíček, Jan
Maixner, Jaroslav
Pažout, Richard
Hušák, Michal
Cibulková, Jana
Kratochvíl, Bohumil
Alaptide from synchrotron powder diffraction data
title Alaptide from synchrotron powder diffraction data
title_full Alaptide from synchrotron powder diffraction data
title_fullStr Alaptide from synchrotron powder diffraction data
title_full_unstemmed Alaptide from synchrotron powder diffraction data
title_short Alaptide from synchrotron powder diffraction data
title_sort alaptide from synchrotron powder diffraction data
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983785/
https://www.ncbi.nlm.nih.gov/pubmed/21580652
http://dx.doi.org/10.1107/S1600536810007750
work_keys_str_mv AT rohlicekjan alaptidefromsynchrotronpowderdiffractiondata
AT maixnerjaroslav alaptidefromsynchrotronpowderdiffractiondata
AT pazoutrichard alaptidefromsynchrotronpowderdiffractiondata
AT husakmichal alaptidefromsynchrotronpowderdiffractiondata
AT cibulkovajana alaptidefromsynchrotronpowderdiffractiondata
AT kratochvilbohumil alaptidefromsynchrotronpowderdiffractiondata

Ejemplares similares