N′-(3-Methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate

There are two independent formula units in the asymmetric unit of the title compound, C(15)H(13)N(3)O(4)·H(2)O. The C=C—N—C torsion angle of the methyl­idenehydrazide group is 174.3 (2)° in one mol­ecule and 178.6 (2)° in the other. The dihedral angles between the two benzene rings in the two mol­ec...

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Autores principales: Ahmad, Tanveer, Zia-ur-Rehman, Muhammad, Siddiqui, Hamid Latif, Fasih Ullah, Muhammad, Parvez, Masood
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983820/
https://www.ncbi.nlm.nih.gov/pubmed/21580775
http://dx.doi.org/10.1107/S1600536810010986
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author Ahmad, Tanveer
Zia-ur-Rehman, Muhammad
Siddiqui, Hamid Latif
Fasih Ullah, Muhammad
Parvez, Masood
author_facet Ahmad, Tanveer
Zia-ur-Rehman, Muhammad
Siddiqui, Hamid Latif
Fasih Ullah, Muhammad
Parvez, Masood
author_sort Ahmad, Tanveer
collection PubMed
description There are two independent formula units in the asymmetric unit of the title compound, C(15)H(13)N(3)O(4)·H(2)O. The C=C—N—C torsion angle of the methyl­idenehydrazide group is 174.3 (2)° in one mol­ecule and 178.6 (2)° in the other. The dihedral angles between the two benzene rings in the two mol­ecules are 4.17 (12) and 3.58 (12)°. In the crystal structure, inter­molecular O—H⋯O, N—H⋯O and O—H⋯N hydrogen bonds link the components into a two-dimensional network and additional stabilization is provided by weak inter­molecular C—H⋯O hydrogen bonds.
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spelling pubmed-29838202010-12-30 N′-(3-Methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate Ahmad, Tanveer Zia-ur-Rehman, Muhammad Siddiqui, Hamid Latif Fasih Ullah, Muhammad Parvez, Masood Acta Crystallogr Sect E Struct Rep Online Organic Papers There are two independent formula units in the asymmetric unit of the title compound, C(15)H(13)N(3)O(4)·H(2)O. The C=C—N—C torsion angle of the methyl­idenehydrazide group is 174.3 (2)° in one mol­ecule and 178.6 (2)° in the other. The dihedral angles between the two benzene rings in the two mol­ecules are 4.17 (12) and 3.58 (12)°. In the crystal structure, inter­molecular O—H⋯O, N—H⋯O and O—H⋯N hydrogen bonds link the components into a two-dimensional network and additional stabilization is provided by weak inter­molecular C—H⋯O hydrogen bonds. International Union of Crystallography 2010-03-31 /pmc/articles/PMC2983820/ /pubmed/21580775 http://dx.doi.org/10.1107/S1600536810010986 Text en © Ahmad et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ahmad, Tanveer
Zia-ur-Rehman, Muhammad
Siddiqui, Hamid Latif
Fasih Ullah, Muhammad
Parvez, Masood
N′-(3-Methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate
title N′-(3-Methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate
title_full N′-(3-Methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate
title_fullStr N′-(3-Methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate
title_full_unstemmed N′-(3-Methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate
title_short N′-(3-Methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate
title_sort n′-(3-methoxy­benzyl­idene)-4-nitro­benzohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983820/
https://www.ncbi.nlm.nih.gov/pubmed/21580775
http://dx.doi.org/10.1107/S1600536810010986
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