Ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate

In the title compound, C(11)H(14)N(2)O(5), the mol­ecular structure is stabilized by an intra­molecular N—H⋯O hydrogen bond, which generates an S(6) ring motif. The nitro group is twisted slightly from the attached benzene ring, forming a dihedral angle of 5.2 (2)°. In the crystal packing, inter­mol...

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Autores principales: Abdul Rahim, Aisyah Saad, Abd Hamid, Shafida, Narendra Babu, Shivanagere Nagojappa, Loh, Wan-Sin, Fun, Hoong-Kun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983846/
https://www.ncbi.nlm.nih.gov/pubmed/21580671
http://dx.doi.org/10.1107/S1600536810008147
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author Abdul Rahim, Aisyah Saad
Abd Hamid, Shafida
Narendra Babu, Shivanagere Nagojappa
Loh, Wan-Sin
Fun, Hoong-Kun
author_facet Abdul Rahim, Aisyah Saad
Abd Hamid, Shafida
Narendra Babu, Shivanagere Nagojappa
Loh, Wan-Sin
Fun, Hoong-Kun
author_sort Abdul Rahim, Aisyah Saad
collection PubMed
description In the title compound, C(11)H(14)N(2)O(5), the mol­ecular structure is stabilized by an intra­molecular N—H⋯O hydrogen bond, which generates an S(6) ring motif. The nitro group is twisted slightly from the attached benzene ring, forming a dihedral angle of 5.2 (2)°. In the crystal packing, inter­molecular O—H⋯O and C—H⋯O hydrogen bonds link the mol­ecules into a three-dimensional network. The crystal studied was a non-merohedral twin, the refined ratio of the twin components being 0.264 (2):0.736 (2).
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spelling pubmed-29838462010-12-30 Ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate Abdul Rahim, Aisyah Saad Abd Hamid, Shafida Narendra Babu, Shivanagere Nagojappa Loh, Wan-Sin Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(11)H(14)N(2)O(5), the mol­ecular structure is stabilized by an intra­molecular N—H⋯O hydrogen bond, which generates an S(6) ring motif. The nitro group is twisted slightly from the attached benzene ring, forming a dihedral angle of 5.2 (2)°. In the crystal packing, inter­molecular O—H⋯O and C—H⋯O hydrogen bonds link the mol­ecules into a three-dimensional network. The crystal studied was a non-merohedral twin, the refined ratio of the twin components being 0.264 (2):0.736 (2). International Union of Crystallography 2010-03-17 /pmc/articles/PMC2983846/ /pubmed/21580671 http://dx.doi.org/10.1107/S1600536810008147 Text en © Rahim et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Abdul Rahim, Aisyah Saad
Abd Hamid, Shafida
Narendra Babu, Shivanagere Nagojappa
Loh, Wan-Sin
Fun, Hoong-Kun
Ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate
title Ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate
title_full Ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate
title_fullStr Ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate
title_full_unstemmed Ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate
title_short Ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate
title_sort ethyl 4-(2-hydroxy­ethyl­amino)-3-nitro­benzoate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983846/
https://www.ncbi.nlm.nih.gov/pubmed/21580671
http://dx.doi.org/10.1107/S1600536810008147
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