2-Amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph

The title salt, C(6)H(9)N(2) (+)·C(2)F(3)O(2) (−), is a monoclinic polymorph of a previously reported structure [Hemamalini & Fun (2010). Acta Cryst. E66, o781–o782]. In the crystal structure, the cations and anions are linked by two different types of N—H⋯O hydrogen bonds, forming cation–anion...

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Autores principales: Pourayoubi, Mehrdad, Toghraee, Maryam, Rheingold, Arnold L., Golen, James A.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983996/
https://www.ncbi.nlm.nih.gov/pubmed/21580669
http://dx.doi.org/10.1107/S1600536810008408
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author Pourayoubi, Mehrdad
Toghraee, Maryam
Rheingold, Arnold L.
Golen, James A.
author_facet Pourayoubi, Mehrdad
Toghraee, Maryam
Rheingold, Arnold L.
Golen, James A.
author_sort Pourayoubi, Mehrdad
collection PubMed
description The title salt, C(6)H(9)N(2) (+)·C(2)F(3)O(2) (−), is a monoclinic polymorph of a previously reported structure [Hemamalini & Fun (2010). Acta Cryst. E66, o781–o782]. In the crystal structure, the cations and anions are linked by two different types of N—H⋯O hydrogen bonds, forming cation–anion pairs. These pairs are hydrogen bonded to neighbouring pairs via another N—H⋯O hydrogen bonds involving an H atom of the NH(2) group and one of the O atoms of the COO(−) group into a chain extended along the b axis.
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spelling pubmed-29839962010-12-30 2-Amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph Pourayoubi, Mehrdad Toghraee, Maryam Rheingold, Arnold L. Golen, James A. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title salt, C(6)H(9)N(2) (+)·C(2)F(3)O(2) (−), is a monoclinic polymorph of a previously reported structure [Hemamalini & Fun (2010). Acta Cryst. E66, o781–o782]. In the crystal structure, the cations and anions are linked by two different types of N—H⋯O hydrogen bonds, forming cation–anion pairs. These pairs are hydrogen bonded to neighbouring pairs via another N—H⋯O hydrogen bonds involving an H atom of the NH(2) group and one of the O atoms of the COO(−) group into a chain extended along the b axis. International Union of Crystallography 2010-03-17 /pmc/articles/PMC2983996/ /pubmed/21580669 http://dx.doi.org/10.1107/S1600536810008408 Text en © Pourayoubi et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Pourayoubi, Mehrdad
Toghraee, Maryam
Rheingold, Arnold L.
Golen, James A.
2-Amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph
title 2-Amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph
title_full 2-Amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph
title_fullStr 2-Amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph
title_full_unstemmed 2-Amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph
title_short 2-Amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph
title_sort 2-amino-4-methyl­pyridinium trifluoro­acetate: a monoclinic polymorph
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2983996/
https://www.ncbi.nlm.nih.gov/pubmed/21580669
http://dx.doi.org/10.1107/S1600536810008408
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AT toghraeemaryam 2amino4methylpyridiniumtrifluoroacetateamonoclinicpolymorph
AT rheingoldarnoldl 2amino4methylpyridiniumtrifluoroacetateamonoclinicpolymorph
AT golenjamesa 2amino4methylpyridiniumtrifluoroacetateamonoclinicpolymorph

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