(3S,NR)-3-Hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1)

In the title compound, C(16)H(24)NO(+)·Br(−)·C(20)H(14)O(2), the N-hetero­cyclic six-membered ring assumes a half-chair conformation. The two naphthalene ring systems are nearly perpendicular to one another, making a dihedral angle of 89.5 (2)°. Inter­molecular O—H⋯Br hydrogen bonding helps to stabi...

Descripción completa

Detalles Bibliográficos
Autores principales: Wu, Xiao-Qing, Huang, Qing-Chun, Chen, Xiao-Zhen, Li, Guo-You, Zhang, Guo-Lin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2984017/
https://www.ncbi.nlm.nih.gov/pubmed/21580612
http://dx.doi.org/10.1107/S1600536810007944
_version_ 1782192014066974720
author Wu, Xiao-Qing
Huang, Qing-Chun
Chen, Xiao-Zhen
Li, Guo-You
Zhang, Guo-Lin
author_facet Wu, Xiao-Qing
Huang, Qing-Chun
Chen, Xiao-Zhen
Li, Guo-You
Zhang, Guo-Lin
author_sort Wu, Xiao-Qing
collection PubMed
description In the title compound, C(16)H(24)NO(+)·Br(−)·C(20)H(14)O(2), the N-hetero­cyclic six-membered ring assumes a half-chair conformation. The two naphthalene ring systems are nearly perpendicular to one another, making a dihedral angle of 89.5 (2)°. Inter­molecular O—H⋯Br hydrogen bonding helps to stabilize the crystal structure.
format Text
id pubmed-2984017
institution National Center for Biotechnology Information
language English
publishDate 2010
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29840172010-12-30 (3S,NR)-3-Hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1) Wu, Xiao-Qing Huang, Qing-Chun Chen, Xiao-Zhen Li, Guo-You Zhang, Guo-Lin Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(24)NO(+)·Br(−)·C(20)H(14)O(2), the N-hetero­cyclic six-membered ring assumes a half-chair conformation. The two naphthalene ring systems are nearly perpendicular to one another, making a dihedral angle of 89.5 (2)°. Inter­molecular O—H⋯Br hydrogen bonding helps to stabilize the crystal structure. International Union of Crystallography 2010-03-06 /pmc/articles/PMC2984017/ /pubmed/21580612 http://dx.doi.org/10.1107/S1600536810007944 Text en © Wu et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wu, Xiao-Qing
Huang, Qing-Chun
Chen, Xiao-Zhen
Li, Guo-You
Zhang, Guo-Lin
(3S,NR)-3-Hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1)
title (3S,NR)-3-Hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1)
title_full (3S,NR)-3-Hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1)
title_fullStr (3S,NR)-3-Hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1)
title_full_unstemmed (3S,NR)-3-Hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1)
title_short (3S,NR)-3-Hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1)
title_sort (3s,nr)-3-hydroxy­methyl-2-methyl-2-(3-methyl­but-2-en-1-yl)-1,2,3,4-tetra­hydro­isoquinolinium bromide–1,1′-bi-2-naphthol (1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2984017/
https://www.ncbi.nlm.nih.gov/pubmed/21580612
http://dx.doi.org/10.1107/S1600536810007944
work_keys_str_mv AT wuxiaoqing 3snr3hydroxymethyl2methyl23methylbut2en1yl1234tetrahydroisoquinoliniumbromide11bi2naphthol11
AT huangqingchun 3snr3hydroxymethyl2methyl23methylbut2en1yl1234tetrahydroisoquinoliniumbromide11bi2naphthol11
AT chenxiaozhen 3snr3hydroxymethyl2methyl23methylbut2en1yl1234tetrahydroisoquinoliniumbromide11bi2naphthol11
AT liguoyou 3snr3hydroxymethyl2methyl23methylbut2en1yl1234tetrahydroisoquinoliniumbromide11bi2naphthol11
AT zhangguolin 3snr3hydroxymethyl2methyl23methylbut2en1yl1234tetrahydroisoquinoliniumbromide11bi2naphthol11

Ejemplares similares