N-(3-Chloro­phen­yl)-3-methyl­benzamide hemihydrate

In the title compound, C(14)H(12)ClNO·0.5H(2)O, the N—H bond is in an anti conformation to the C=O bond. The two aromatic rings make a dihedral angle of 49.5 (1)°. The water mol­ecule lies on a twofold rotation axis. In the crystal, inter­molecular N—H⋯O and O—H⋯O hydrogen bonds connect the mol­ecul...

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Autores principales: Rodrigues, Vinola Zeena, Tokarčík, Miroslav, Gowda, B. Thimme, Kožíšek, Jozef
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2984021/
https://www.ncbi.nlm.nih.gov/pubmed/21580793
http://dx.doi.org/10.1107/S1600536810010354
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author Rodrigues, Vinola Zeena
Tokarčík, Miroslav
Gowda, B. Thimme
Kožíšek, Jozef
author_facet Rodrigues, Vinola Zeena
Tokarčík, Miroslav
Gowda, B. Thimme
Kožíšek, Jozef
author_sort Rodrigues, Vinola Zeena
collection PubMed
description In the title compound, C(14)H(12)ClNO·0.5H(2)O, the N—H bond is in an anti conformation to the C=O bond. The two aromatic rings make a dihedral angle of 49.5 (1)°. The water mol­ecule lies on a twofold rotation axis. In the crystal, inter­molecular N—H⋯O and O—H⋯O hydrogen bonds connect the mol­ecules into a three-dimensional network.
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spelling pubmed-29840212010-12-30 N-(3-Chloro­phen­yl)-3-methyl­benzamide hemihydrate Rodrigues, Vinola Zeena Tokarčík, Miroslav Gowda, B. Thimme Kožíšek, Jozef Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(12)ClNO·0.5H(2)O, the N—H bond is in an anti conformation to the C=O bond. The two aromatic rings make a dihedral angle of 49.5 (1)°. The water mol­ecule lies on a twofold rotation axis. In the crystal, inter­molecular N—H⋯O and O—H⋯O hydrogen bonds connect the mol­ecules into a three-dimensional network. International Union of Crystallography 2010-03-31 /pmc/articles/PMC2984021/ /pubmed/21580793 http://dx.doi.org/10.1107/S1600536810010354 Text en © Rodrigues et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Rodrigues, Vinola Zeena
Tokarčík, Miroslav
Gowda, B. Thimme
Kožíšek, Jozef
N-(3-Chloro­phen­yl)-3-methyl­benzamide hemihydrate
title N-(3-Chloro­phen­yl)-3-methyl­benzamide hemihydrate
title_full N-(3-Chloro­phen­yl)-3-methyl­benzamide hemihydrate
title_fullStr N-(3-Chloro­phen­yl)-3-methyl­benzamide hemihydrate
title_full_unstemmed N-(3-Chloro­phen­yl)-3-methyl­benzamide hemihydrate
title_short N-(3-Chloro­phen­yl)-3-methyl­benzamide hemihydrate
title_sort n-(3-chloro­phen­yl)-3-methyl­benzamide hemihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2984021/
https://www.ncbi.nlm.nih.gov/pubmed/21580793
http://dx.doi.org/10.1107/S1600536810010354
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AT kozisekjozef n3chlorophenyl3methylbenzamidehemihydrate

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