N′-(2-Hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide

The title compound, C(14)H(13)N(3)O(3), was synthesized by the condensation reaction of 2-hydr­oxy-4-methoxy­benzaldehyde with isonicotinohydrazide in a methanol solution. The mol­ecule of the compound displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between t...

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Detalles Bibliográficos
Autores principales: Zhi, Feng, Wang, Rong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2984034/
https://www.ncbi.nlm.nih.gov/pubmed/21580709
http://dx.doi.org/10.1107/S1600536810010020
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author Zhi, Feng
Wang, Rong
author_facet Zhi, Feng
Wang, Rong
author_sort Zhi, Feng
collection PubMed
description The title compound, C(14)H(13)N(3)O(3), was synthesized by the condensation reaction of 2-hydr­oxy-4-methoxy­benzaldehyde with isonicotinohydrazide in a methanol solution. The mol­ecule of the compound displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between the benzene and the pyridine rings is 27.3 (2)°. In the crystal, mol­ecules are linked by N—H⋯N inter­actions into zigzag chains with graph-set notation C(7) along [010]. An intra­molecular O—H⋯N hydrogen bond is observed.
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spelling pubmed-29840342010-12-30 N′-(2-Hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide Zhi, Feng Wang, Rong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(13)N(3)O(3), was synthesized by the condensation reaction of 2-hydr­oxy-4-methoxy­benzaldehyde with isonicotinohydrazide in a methanol solution. The mol­ecule of the compound displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between the benzene and the pyridine rings is 27.3 (2)°. In the crystal, mol­ecules are linked by N—H⋯N inter­actions into zigzag chains with graph-set notation C(7) along [010]. An intra­molecular O—H⋯N hydrogen bond is observed. International Union of Crystallography 2010-03-20 /pmc/articles/PMC2984034/ /pubmed/21580709 http://dx.doi.org/10.1107/S1600536810010020 Text en © Zhi and Wang 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhi, Feng
Wang, Rong
N′-(2-Hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide
title N′-(2-Hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide
title_full N′-(2-Hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide
title_fullStr N′-(2-Hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide
title_full_unstemmed N′-(2-Hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide
title_short N′-(2-Hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide
title_sort n′-(2-hydr­oxy-4-methoxy­benzyl­idene)isonicotinohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2984034/
https://www.ncbi.nlm.nih.gov/pubmed/21580709
http://dx.doi.org/10.1107/S1600536810010020
work_keys_str_mv AT zhifeng n2hydroxy4methoxybenzylideneisonicotinohydrazide
AT wangrong n2hydroxy4methoxybenzylideneisonicotinohydrazide

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