6-Chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1H)-one

The asymmetric unit of the title quinazolinone compound, C(16)H(13)ClN(2)OS, consists of two crystallographically independent mol­ecules, A and B. The dihedral angles between the quinazoline and benzene rings are 16.88 (6) and 32.34 (6)° for mol­ecules A and B, respectively. In the crystal structure...

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Autores principales: Hashim, Norhafizah Mohd, Osman, Hasnah, Rahim, Afidah Abdul, Yeap, Chin Sing, Fun, Hoong-Kun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2984037/
https://www.ncbi.nlm.nih.gov/pubmed/21580754
http://dx.doi.org/10.1107/S1600536810010330
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author Hashim, Norhafizah Mohd
Osman, Hasnah
Rahim, Afidah Abdul
Yeap, Chin Sing
Fun, Hoong-Kun
author_facet Hashim, Norhafizah Mohd
Osman, Hasnah
Rahim, Afidah Abdul
Yeap, Chin Sing
Fun, Hoong-Kun
author_sort Hashim, Norhafizah Mohd
collection PubMed
description The asymmetric unit of the title quinazolinone compound, C(16)H(13)ClN(2)OS, consists of two crystallographically independent mol­ecules, A and B. The dihedral angles between the quinazoline and benzene rings are 16.88 (6) and 32.34 (6)° for mol­ecules A and B, respectively. In the crystal structure, mol­ecules A and B are linked by two bifurcated inter­molecular N—H⋯S and C—H⋯S hydrogen bonds. Pairs of mol­ecules are further linked by C—H⋯O and C—H⋯Cl hydrogen bonds into a chain aligned approximately along [110].
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spelling pubmed-29840372010-12-30 6-Chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1H)-one Hashim, Norhafizah Mohd Osman, Hasnah Rahim, Afidah Abdul Yeap, Chin Sing Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title quinazolinone compound, C(16)H(13)ClN(2)OS, consists of two crystallographically independent mol­ecules, A and B. The dihedral angles between the quinazoline and benzene rings are 16.88 (6) and 32.34 (6)° for mol­ecules A and B, respectively. In the crystal structure, mol­ecules A and B are linked by two bifurcated inter­molecular N—H⋯S and C—H⋯S hydrogen bonds. Pairs of mol­ecules are further linked by C—H⋯O and C—H⋯Cl hydrogen bonds into a chain aligned approximately along [110]. International Union of Crystallography 2010-03-27 /pmc/articles/PMC2984037/ /pubmed/21580754 http://dx.doi.org/10.1107/S1600536810010330 Text en © Hashim et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hashim, Norhafizah Mohd
Osman, Hasnah
Rahim, Afidah Abdul
Yeap, Chin Sing
Fun, Hoong-Kun
6-Chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1H)-one
title 6-Chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1H)-one
title_full 6-Chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1H)-one
title_fullStr 6-Chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1H)-one
title_full_unstemmed 6-Chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1H)-one
title_short 6-Chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1H)-one
title_sort 6-chloro-3-phenethyl-2-thioxo-2,3-di­hydro­quinazolin-4(1h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2984037/
https://www.ncbi.nlm.nih.gov/pubmed/21580754
http://dx.doi.org/10.1107/S1600536810010330
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