10-Hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10H)-one

In the title phenanthrenone compound, C(18)H(13)NO(2)S, the dihydro­phenanthrene ring system is not planar, with its central ring distorted to a screw-boat conformation. The essentially planar thia­zole ring [maximum deviation = 0.005 (1) Å] is inclined at an inter­planar angle of 23.36 (5)° with re...

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Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Goh, Jia Hao, Liu, Yang, Zhang, Yan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006705/
https://www.ncbi.nlm.nih.gov/pubmed/21587908
http://dx.doi.org/10.1107/S1600536810022439
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author Fun, Hoong-Kun
Goh, Jia Hao
Liu, Yang
Zhang, Yan
author_facet Fun, Hoong-Kun
Goh, Jia Hao
Liu, Yang
Zhang, Yan
author_sort Fun, Hoong-Kun
collection PubMed
description In the title phenanthrenone compound, C(18)H(13)NO(2)S, the dihydro­phenanthrene ring system is not planar, with its central ring distorted to a screw-boat conformation. The essentially planar thia­zole ring [maximum deviation = 0.005 (1) Å] is inclined at an inter­planar angle of 23.36 (5)° with respect to the mean plane through the dihydro­phenanthrene ring system. In the crystal packing, inter­molecular O—H⋯N hydrogen bonds link the mol­ecules into infinite chains along the a axis. Weak inter­molecular C—H⋯π inter­actions further stabilize the crystal packing.
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spelling pubmed-30067052010-12-30 10-Hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10H)-one Fun, Hoong-Kun Goh, Jia Hao Liu, Yang Zhang, Yan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title phenanthrenone compound, C(18)H(13)NO(2)S, the dihydro­phenanthrene ring system is not planar, with its central ring distorted to a screw-boat conformation. The essentially planar thia­zole ring [maximum deviation = 0.005 (1) Å] is inclined at an inter­planar angle of 23.36 (5)° with respect to the mean plane through the dihydro­phenanthrene ring system. In the crystal packing, inter­molecular O—H⋯N hydrogen bonds link the mol­ecules into infinite chains along the a axis. Weak inter­molecular C—H⋯π inter­actions further stabilize the crystal packing. International Union of Crystallography 2010-06-16 /pmc/articles/PMC3006705/ /pubmed/21587908 http://dx.doi.org/10.1107/S1600536810022439 Text en © Fun et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Goh, Jia Hao
Liu, Yang
Zhang, Yan
10-Hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10H)-one
title 10-Hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10H)-one
title_full 10-Hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10H)-one
title_fullStr 10-Hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10H)-one
title_full_unstemmed 10-Hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10H)-one
title_short 10-Hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10H)-one
title_sort 10-hy­droxy-10-(1,3-thia­zol-2-ylmeth­yl)phenanthren-9(10h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006705/
https://www.ncbi.nlm.nih.gov/pubmed/21587908
http://dx.doi.org/10.1107/S1600536810022439
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AT zhangyan 10hydroxy1013thiazol2ylmethylphenanthren910hone

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