2,2-Bis(hy­droxy­meth­yl)-2,3-dihydro-1H-pyrrolizin-1-one

The title compound, C(9)H(11)NO(3), was prepared by an Aldol reaction of 2,3-dihydro-1H-pyrrolizin-1-one with formaldehyde. The asymmetric unit contains six mol­ecules. The pyrrolizine ring system in each mol­ecule is planar, the maximum atomic deviation being 0.066 (2) Å. In the crystal structure,...

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Detalles Bibliográficos
Autores principales: Ali, Yousuf, Peng, Yu, Hua, Erbing, Afza, Nighat, Khan, Rashid Ali
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006763/
https://www.ncbi.nlm.nih.gov/pubmed/21587820
http://dx.doi.org/10.1107/S1600536810018970
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author Ali, Yousuf
Peng, Yu
Hua, Erbing
Afza, Nighat
Khan, Rashid Ali
author_facet Ali, Yousuf
Peng, Yu
Hua, Erbing
Afza, Nighat
Khan, Rashid Ali
author_sort Ali, Yousuf
collection PubMed
description The title compound, C(9)H(11)NO(3), was prepared by an Aldol reaction of 2,3-dihydro-1H-pyrrolizin-1-one with formaldehyde. The asymmetric unit contains six mol­ecules. The pyrrolizine ring system in each mol­ecule is planar, the maximum atomic deviation being 0.066 (2) Å. In the crystal structure, mol­ecules are liked together by an extensive O—H⋯O hydrogen-bonding network.
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spelling pubmed-30067632010-12-30 2,2-Bis(hy­droxy­meth­yl)-2,3-dihydro-1H-pyrrolizin-1-one Ali, Yousuf Peng, Yu Hua, Erbing Afza, Nighat Khan, Rashid Ali Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(9)H(11)NO(3), was prepared by an Aldol reaction of 2,3-dihydro-1H-pyrrolizin-1-one with formaldehyde. The asymmetric unit contains six mol­ecules. The pyrrolizine ring system in each mol­ecule is planar, the maximum atomic deviation being 0.066 (2) Å. In the crystal structure, mol­ecules are liked together by an extensive O—H⋯O hydrogen-bonding network. International Union of Crystallography 2010-06-05 /pmc/articles/PMC3006763/ /pubmed/21587820 http://dx.doi.org/10.1107/S1600536810018970 Text en © Ali et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ali, Yousuf
Peng, Yu
Hua, Erbing
Afza, Nighat
Khan, Rashid Ali
2,2-Bis(hy­droxy­meth­yl)-2,3-dihydro-1H-pyrrolizin-1-one
title 2,2-Bis(hy­droxy­meth­yl)-2,3-dihydro-1H-pyrrolizin-1-one
title_full 2,2-Bis(hy­droxy­meth­yl)-2,3-dihydro-1H-pyrrolizin-1-one
title_fullStr 2,2-Bis(hy­droxy­meth­yl)-2,3-dihydro-1H-pyrrolizin-1-one
title_full_unstemmed 2,2-Bis(hy­droxy­meth­yl)-2,3-dihydro-1H-pyrrolizin-1-one
title_short 2,2-Bis(hy­droxy­meth­yl)-2,3-dihydro-1H-pyrrolizin-1-one
title_sort 2,2-bis(hy­droxy­meth­yl)-2,3-dihydro-1h-pyrrolizin-1-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006763/
https://www.ncbi.nlm.nih.gov/pubmed/21587820
http://dx.doi.org/10.1107/S1600536810018970
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