8b,8c-Diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate

In the thio­glycoluril system of the title compound, C(32)H(30)N(8)S(2)·CHCl(3), the two pyridine rings are roughly parallel, forming a dihedral angle of 7.2 (1)°, and the distance between the centroids of the two phenyl rings is 3.951 (5) Å. The chloro­form solvent mol­ecule is linked to the main m...

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Detalles Bibliográficos
Autores principales: Deng, Cong, Shu, Wenming, Zhang, Dongxue
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006766/
https://www.ncbi.nlm.nih.gov/pubmed/21587774
http://dx.doi.org/10.1107/S1600536810020040
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author Deng, Cong
Shu, Wenming
Zhang, Dongxue
author_facet Deng, Cong
Shu, Wenming
Zhang, Dongxue
author_sort Deng, Cong
collection PubMed
description In the thio­glycoluril system of the title compound, C(32)H(30)N(8)S(2)·CHCl(3), the two pyridine rings are roughly parallel, forming a dihedral angle of 7.2 (1)°, and the distance between the centroids of the two phenyl rings is 3.951 (5) Å. The chloro­form solvent mol­ecule is linked to the main mol­ecule via a weak C—H⋯N hydrogen bond.
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spelling pubmed-30067662010-12-30 8b,8c-Diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate Deng, Cong Shu, Wenming Zhang, Dongxue Acta Crystallogr Sect E Struct Rep Online Organic Papers In the thio­glycoluril system of the title compound, C(32)H(30)N(8)S(2)·CHCl(3), the two pyridine rings are roughly parallel, forming a dihedral angle of 7.2 (1)°, and the distance between the centroids of the two phenyl rings is 3.951 (5) Å. The chloro­form solvent mol­ecule is linked to the main mol­ecule via a weak C—H⋯N hydrogen bond. International Union of Crystallography 2010-06-05 /pmc/articles/PMC3006766/ /pubmed/21587774 http://dx.doi.org/10.1107/S1600536810020040 Text en © Deng et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Deng, Cong
Shu, Wenming
Zhang, Dongxue
8b,8c-Diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate
title 8b,8c-Diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate
title_full 8b,8c-Diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate
title_fullStr 8b,8c-Diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate
title_full_unstemmed 8b,8c-Diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate
title_short 8b,8c-Diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate
title_sort 8b,8c-diphenyl-2,6-bis(4-pyridyl­meth­yl)­perhydro-2,3a,4a,6,7a,8a-hexa­aza­cyclo­penta­[def]fluorene-4,8-dithione chloro­form solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006766/
https://www.ncbi.nlm.nih.gov/pubmed/21587774
http://dx.doi.org/10.1107/S1600536810020040
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