N′-(5-Chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide

The title Schiff base compound, C(15)H(13)ClN(2)O(3), was prepared by the reaction of equimolar quanti­ties of 5-chloro-2-hy­droxy­benzaldehyde with 2-meth­oxy­benzohydrazide in a methanol solution. The dihedral angle between the two benzene rings is 20.6 (3)°. An intra­molecular O—H⋯N hydrogen bond...

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Autor principal: Hao, Yu-Mei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006787/
https://www.ncbi.nlm.nih.gov/pubmed/21587862
http://dx.doi.org/10.1107/S160053681002180X
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author Hao, Yu-Mei
author_facet Hao, Yu-Mei
author_sort Hao, Yu-Mei
collection PubMed
description The title Schiff base compound, C(15)H(13)ClN(2)O(3), was prepared by the reaction of equimolar quanti­ties of 5-chloro-2-hy­droxy­benzaldehyde with 2-meth­oxy­benzohydrazide in a methanol solution. The dihedral angle between the two benzene rings is 20.6 (3)°. An intra­molecular O—H⋯N hydrogen bond may influence the mol­ecular conformation. In the crystal structure, mol­ecules form chains along the b direction via inter­molecular N—H⋯O hydrogen bonds which are bifurcated involving an intra­molecular N—H⋯O hydrogen bond.
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spelling pubmed-30067872010-12-30 N′-(5-Chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide Hao, Yu-Mei Acta Crystallogr Sect E Struct Rep Online Organic Papers The title Schiff base compound, C(15)H(13)ClN(2)O(3), was prepared by the reaction of equimolar quanti­ties of 5-chloro-2-hy­droxy­benzaldehyde with 2-meth­oxy­benzohydrazide in a methanol solution. The dihedral angle between the two benzene rings is 20.6 (3)°. An intra­molecular O—H⋯N hydrogen bond may influence the mol­ecular conformation. In the crystal structure, mol­ecules form chains along the b direction via inter­molecular N—H⋯O hydrogen bonds which are bifurcated involving an intra­molecular N—H⋯O hydrogen bond. International Union of Crystallography 2010-06-16 /pmc/articles/PMC3006787/ /pubmed/21587862 http://dx.doi.org/10.1107/S160053681002180X Text en © Yu-Mei Hao 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hao, Yu-Mei
N′-(5-Chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide
title N′-(5-Chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide
title_full N′-(5-Chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide
title_fullStr N′-(5-Chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide
title_full_unstemmed N′-(5-Chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide
title_short N′-(5-Chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide
title_sort n′-(5-chloro-2-hy­droxy­benzyl­idene)-2-meth­oxy­benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006787/
https://www.ncbi.nlm.nih.gov/pubmed/21587862
http://dx.doi.org/10.1107/S160053681002180X
work_keys_str_mv AT haoyumei n5chloro2hydroxybenzylidene2methoxybenzohydrazide

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