1-[1-(4-Bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide

In the title compound, C(17)H(18)BrN(3)O(2)S, the dihedral angle between the aromatic rings is 9.15 (17)°. A bifurcated intra­molecular N—H⋯(N,O) hydrogen bond generates two S(5) rings and a weak intra­molecular C—H⋯S inter­action completes an S(6) ring motif. In the crystal, inversion dimers linked...

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Detalles Bibliográficos
Autores principales: Yaqub, Muhammad, Pervez, Humayun, Arif, Nadia, Tahir, M. Nawaz, Hussain, Mazhar
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006822/
https://www.ncbi.nlm.nih.gov/pubmed/21587917
http://dx.doi.org/10.1107/S1600536810022622
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author Yaqub, Muhammad
Pervez, Humayun
Arif, Nadia
Tahir, M. Nawaz
Hussain, Mazhar
author_facet Yaqub, Muhammad
Pervez, Humayun
Arif, Nadia
Tahir, M. Nawaz
Hussain, Mazhar
author_sort Yaqub, Muhammad
collection PubMed
description In the title compound, C(17)H(18)BrN(3)O(2)S, the dihedral angle between the aromatic rings is 9.15 (17)°. A bifurcated intra­molecular N—H⋯(N,O) hydrogen bond generates two S(5) rings and a weak intra­molecular C—H⋯S inter­action completes an S(6) ring motif. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops and weak C—H⋯S and C—H⋯π inter­actions are also present.
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spelling pubmed-30068222010-12-30 1-[1-(4-Bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide Yaqub, Muhammad Pervez, Humayun Arif, Nadia Tahir, M. Nawaz Hussain, Mazhar Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(17)H(18)BrN(3)O(2)S, the dihedral angle between the aromatic rings is 9.15 (17)°. A bifurcated intra­molecular N—H⋯(N,O) hydrogen bond generates two S(5) rings and a weak intra­molecular C—H⋯S inter­action completes an S(6) ring motif. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops and weak C—H⋯S and C—H⋯π inter­actions are also present. International Union of Crystallography 2010-06-18 /pmc/articles/PMC3006822/ /pubmed/21587917 http://dx.doi.org/10.1107/S1600536810022622 Text en © Yaqub et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yaqub, Muhammad
Pervez, Humayun
Arif, Nadia
Tahir, M. Nawaz
Hussain, Mazhar
1-[1-(4-Bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide
title 1-[1-(4-Bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide
title_full 1-[1-(4-Bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide
title_fullStr 1-[1-(4-Bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide
title_full_unstemmed 1-[1-(4-Bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide
title_short 1-[1-(4-Bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide
title_sort 1-[1-(4-bromo­phen­yl)ethyl­idene]-4-(2,4-dimeth­oxy­phen­yl)thio­semicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006822/
https://www.ncbi.nlm.nih.gov/pubmed/21587917
http://dx.doi.org/10.1107/S1600536810022622
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